African Mineral Standards

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1 Tel: ax: web: 30 lectron Avenue, sando, P.O. ox 856, sando, 1600, South Africa. A Division of Set Point ndustrial Technology ( Pty ) Ltd. Reg.No. 1989/000201/07. African Mineral Standards Nickel-Copper Sulphide Standard Nkomati Mine South Africa AMS0073 Certificate of Analysis Recommended Concentration and two etween Laboratory Standard Deviations Certified Concentrations conomic lements Co (M/CP) 277 ± 17 ppm Cu (P) 2370 ± 200 ppm Cu (M/CP) 2414 ± 210 ppm Cu (XR) 2454 ± 100 ppm Ni (P) 5316 ± 418 ppm Ni (M/CP) 5459 ± 368 ppm Ni (XR) 5723 ± 212 ppm Pt (Pb Collection) 0.33 ± 0.03 g/t Pd (Pb Collection) 0.89 ± 0.06 g/t Specific Gravity 3.04 ± 0.18 g/cc Major lements Al 2 O ± 0.14 % CaO ± 0.34 % Cr 2 O ± 0.02 % e 2 O ± 0.62 % K 2 O 0.46 ± 0.02 % LO 7.04 ± 0.54 % MgO ± 0.40 % MnO 0.21 ± 0.02 % SiO ± 0.64 % TiO ± 0.02 % Directors: G Horsfield (CO), MD vers (CO)(ritish), ND Kennelly, S ngram, MC Louw, Dr C Rademeyer, N Robinson, M Smith, MH Snelling, Vassiloudis, D Williams

2 Provisional Concentrations conomic lements Au (Pb Collection) ± 0.01 g/t Co (P) 260 ± 40 ppm Co (XR) 315 ± 72 ppm Major lements Na 2 O 0.43 ± 0.06 % P 2 O ± 0.01 % S 4.53 ± 0.70 % ntended use: AMS0073 is suitable for monitoring the accuracy of a single analysis of nickel-copper sulphide ores hosted by mafic-ultramafic rocks. The material can be used for routine quality control by inserting within a batch of samples. The recommended mean and "etween Lab" standard deviations for this standard reflect the average results from the laboratories that participated in the round robin. Slight variations in analytical procedures between laboratories will reflect as slight biases to the recommended concentrations and this is acceptable. Good laboratories however will report results within the two standard deviation levels with a failure of <10 %. Origin of material: The material for this standard was provided by the Nkomati Nickel Mine, a joint venture between ARM Platinum and Norilsk Nickel Africa (Pty) Ltd. The mine is situated in the Machadodorp area, Mpumalanga, approximately 300 km east of ohannesburg in South Africa. Mineral and chemical composition: Minearalisation at Nkomati occurs in a number of distinct zones within the Uitkomst Complex, a layered mafic-ultramafic intrusion exposed in a broad valley dissecting the Transvaal Sequence. conomic sulphide mineralization occurs as disseminations, blebs and stringers in three zones, namely the asal Mineralised Zone (MZ), in the asal Gabbro; the Main Mineralised Zone (MMZ), in the Lower Pyroxenite, and the Chromititic Peridotite Mineralised Zone (PCMZ), in the Chromititic Peridotite. The Massive Sulphide ody (MS), which was situated mainly in the granite basement below the Uitkomst Complex has been mined out. AMS0073 is made from Main Mineralised Zone (MMZ) material, which is a heterogeneous unit consisting mainly of altered pyroxenites and harzburgites with calc-silicate xenoliths. Appearance: The material is a very fine powder coloured lueish Grey (Corstor 5P 5/1). Method of preparation: The material was crushed, dry-milled and air-classified to 100% <54um. Wet sieve particle size analysis of random samples confirmed the material was 100% <54um. t was then blended in a bi-conical mixer, systematically divided and then sealed into 1kg Laboratory Packs. Samples were randomly selected for homogeneity testing and third party analysis. Statistical analysis for the consensus test results were carried out by an independent statistician. xplorer Packs are subdivided from the Laboratory packs as required. 2

3 Methods of analysis requested: 1. Au, Pt, Pd Pb collection CP-OS or CP-MS. 2. Multi-acid digest multi-element scan - ( to include Co, Cu, Ni. ). CP-OS or CP-MS. 3. Aqua regia digest - Co, Cu, Ni. CP-OS or CP-MS. 4. Co, Cu, Ni. XR. 5. Majors ( Al 2 O 3, CaO, Cr 2 O 3, e 2 O 3, K 2 O, MgO, MnO, Na 2 O, SiO 2, TiO 2. LO. ) XR fusion. 6. SG ( gas pycnometer ) Method of certification: Twenty three laboratories were each given eight randomly selected packages of sample. The results from the eighteen laboratories that issued results timeously were used for the certification. ourteen of those laboratories also returned major element data that could be certified and trace element data that was not certified but which is reported as an appendix. The mean and standard deviation for all data was calculated. Outliers were defined as samples beyond the mean ± 2 Standard Deviations from all data. These outliers were removed from the data and a new mean and standard deviation was determined. Standards with an RSD of near or less than 5 % are then certified, RSD s of between near 5 % and 15 % are given Provisional Concentrations and limits, those with RSD s over 15 % are given ndicated Concentrations. This method is different from that used to calculate the Confidence nterval shown on many Government-produced standards in that the actual between-laboratory standard deviation is used in the calculations. This produces upper and lower limits that reflect actual individual analyses rather than a grouped set of analyses. The limits can therefore be used to monitor accuracy from individual analyses, unlike the Certified Limits published on other standards which quote a Confidence nterval. Participating laboratories: (Not in same order as in the table of assays) 1. ACM Analytical Laboratories Ltd CA 2. Activation Laboratories Pty Ltd (ActLabs) CA 3. ALS Chemex Laboratory Group ohannesburg SA 4. ALS Chemex Laboratory Group Perth WA 5. ALS Chemex Laboratory Group Vancouver CA 6. Ammtec Limited WA 7. Anglo Research (Crown Campus) 8. Assayers Canada 9. Geoscience Laboratories (GO LAS) CA 10. ntertek Testing Services Ltd Shanghai (TS eijing) 11. ntertek Utama Services (ndonesia) 12. Labtium nc inland 13. Nkomati V Laboratory SA 14. OMAC Laboratories Limited (reland) 15. Set Point Laboratories (sando) SA 16. SGS Australia Pty Ltd (Newburn) WA 17. SGS Mineral Services Lakefield (Canada) 18. Ultra Trace (Pty) Ltd WA 3

4 Assay Data: Data as received from the laboratories is set out below. A proficiency report has been sent to the managers of the participating laboratories. Lab Au Co Co Co Cu Cu Cu Ni Ni Ni Pd Pt SG Al2O3 CaO Cr2O3 e2o3 K2O LO MgO MnO Na2O P2O5 S SiO2 TiO2 Code g/t ppm ppm ppm ppm ppm ppm ppm ppm ppm g/t g/t g/cc % % % % % % % % % % % % % (PbColl) (M/CP) (P) (XR) (M/CP) (P) (XR) (M/CP) (P) (XR) (PbColl) (PbColl) (XR) (XR) (XR) (XR) (XR) (XR) (XR) (XR) (XR) (XR) (XR) (XR) (XR) A A A A A A A A C C C C C C C C D D D D D D D D G G G G G G G G H H H H H H H H K K K K K K K K L L L L L L L L M M M M M M M M N N N N N N N N

5 Assay Data (cont): Lab Au Co Co Co Cu Cu Cu Ni Ni Ni Pd Pt SG Al2O3 CaO Cr2O3 e2o3 K2O LO MgO MnO Na2O P2O5 S SiO2 TiO2 Code g/t ppm ppm ppm ppm ppm ppm ppm ppm ppm g/t g/t g/cc % % % % % % % % % % % % % (PbColl) (M/CP) (P) (XR) (M/CP) (P) (XR) (M/CP) (P) (XR) (PbColl) (PbColl) (XR) (XR) (XR) (XR) (XR) (XR) (XR) (XR) (XR) (XR) (XR) (XR) (XR) O O O O O O O O P P P P P P P P Q Q Q Q Q Q Q Q R R R R R R R R S S S S S S S S T T T T T T T T U U U U U U U U V V V V V V V V W W W W W W W W Availability: This product is available in Laboratory Packs containing 1kg of material or in xplorer Packs containing client specified weights of material from 50g up to 250g. Laboratory Packs are sealed bottles delivered in sealed foil pouches. xplorer Packs contain material in standard geochem envelopes placed into foil pouches that are nitrogen flushed and vacuum sealed. 5

6 Legal notice: This certificate and the reference material described in it have been prepared with due care and attention. However AMS, Set Point Technology (Pty) Ltd, Mike McWha, Dr arry Smee and Smee and Associates Ltd; accept no liability for any decisions or actions taken following the use of the reference material. 11 August 2008 Certifying officers: African Mineral Standards: Mike McWha Sc (Hons), GSSA, MSAMM, Pr.Sci.Nat Geochemist: arry W. Smee Sc, PhD, P.Geo, (.C.) 6

7 Appendix Additional useful data collected during the round robin exercise includes these iterated but uncertified certified trace element statistics: lement Method Unit Mean 2SD RSD% n Ag M/CP ppm Al M/CP % As M/CP ppm M/CP ppm a M/CP ppm i M/CP ppm Ca M/CP % Cd M/CP ppm Ce M/CP ppm Cr M/CP ppm Cs M/CP ppm e M/CP % Ga M/CP ppm Hf M/CP ppm n M/CP ppm K M/CP % La M/CP ppm Li M/CP ppm Mg M/CP % Mn M/CP ppm Mo M/CP ppm Na M/CP % Nb M/CP ppm P M/CP ppm Pb M/CP ppm Rb M/CP ppm Sb M/CP ppm Sc M/CP ppm Se M/CP ppm Sn M/CP ppm Sr M/CP ppm Ta M/CP ppm Te M/CP ppm Th M/CP ppm Ti M/CP % Tl M/CP ppm U M/CP ppm V M/CP ppm W M/CP ppm Y M/CP ppm Zn M/CP ppm Zr M/CP ppm

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