GC/MS BATCH NUMBER: F80104

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1 GC/MS BATCH NUMBER: F80104 ESSENTIAL OIL: FRANKINCENSE FREREANA BOTANICAL NAME: BOSWELLIA FREREANA ORIGIN: SOMALIA KEY CONSTITUENTS PRESENT IN THIS BATCH OF FRANKINCENSE FREREANA OIL % α-thujene 48.5 α-pinene 15.3 p-cymene 9.3 SABINENE 7.7 LIMONENE 2.5 α-phellandrene 2.3 TERPINEN-4-OL 2.0 β-pinene 2.0 1,8-CINEOLE 1.5 MYRCENE 1.1 Comments from Robert Tisserand: A beautiful incense-y odor quality with hints of Lemon and Tea Tree. Constituents are in expected amounts nd St S. Twin Falls, ID * * planttherapy.com facebook.com/planttherapy * planttherapy.com/blog

2 Date : November 17, 2017 SAMPLE IDENTIFICATION Internal code : 17K14-PTH3-1-CC Customer identification : Frankincense Frereana - Somalia - F R Type : Essential oil Source : Boswellia frereana Customer : Plant Therapy ANALYSIS Method : PC-PA E06, "Analysis of the composition of a liquid essential oil by GC-FID" (in French). Identifications double-checked by GC-MS Analyst : Sylvain Mercier, M. Sc., chimiste Analysis date : Checked and approved by : Alexis St-Gelais, M. Sc., chimiste Note: This report may not be published, including online, without the written consent from Laboratoire PhytoChemia. This report is digitally signed, it is only considered valid if the digital signature is intact. Page 1 of 5

3 IDENTIFIED COMPOUNDS Identification Column: BP5 Column: WAX R.T. R.I. % % R.I. R.T. Molecular Class Toluene * Simple phenolic 2-Isopropylfuran? Furan Unknown (m/z = 93, 91 (68), 121 (60), 77 (50), 79 (43), 105 (21), 41 (20) (17)) Tricyclene 3.22* Monoterpene Hashishene 3.22* 915 [0.10] [64.14] * Monoterpene α-thujene [64.14] * Monoterpene α-pinene [64.14] * Monoterpene Unknown (m/z = 91, 92 (49), 65 (12) ? (2)) * Monoterpene Camphene Monoterpene Thuja-2,4(10)-diene [8.22] * Monoterpene Sabinene [8.22] * Monoterpene β-pinene Monoterpene Myrcene * Monoterpene α-phellandrene 4.76* Monoterpene Δ3-Carene 4.76* 1005 [2.80] Monoterpene α-terpinene [1.72] * Monoterpene meta-cymene [1.72] * Monoterpene para-cymene * Monoterpene Limonene * Monoterpene β-phellandrene [5.13] * Monoterpene 1,8-Cineole [5.13] * Monoterp. ether cis-β-ocimene * Monoterpene trans-β-ocimene [8.41] * Monoterpene Unknown (m/z = 109, 43 (39), 91 (25), 95 (20) Oxygenated monoterpene (15), 137 (19), 152 (1)) γ-terpinene [0.84] * Monoterpene cis-sabinene hydrate Monoterp. alcohol Terpinolene Monoterpene para-cymenene * Monoterpene Linalool Monoterp. alcohol α-thujone [0.15] * Monoterp. ketone β-thujone [0.15] * Monoterp. ketone α-campholenal Monoterp. aldehyde trans-pinocarveol Monoterp. alcohol trans-sabinol Monoterp. alcohol trans-verbenol * Monoterp. alcohol Page 2 of 5

4 α-phellandren-8-ol analog Monoterp. alcohol Pinocarvone Monoterp. ketone Umbellulone Monoterp. ketone α-phellandren-8-ol Monoterp. alcohol Terpinen-4-ol * Monoterp. alcohol Myrtenal [2.41] * Monoterp. aldehyde α-terpineol 9.49* * Monoterp. alcohol β-phellandren-8-ol 9.49* 1204 [0.48] Monoterp. alcohol Verbenone [0.07] * Monoterp. ketone Octyl acetate Aliphatic ester Methyl decyl ether Aliphatic ether Bornyl acetate Monoterp. ester α-cubebene Sesquiterpene α-copaene Sesquiterpene β-bourbonene Sesquiterpene β-cubebene Sesquiterpene β-elemene [2.41] * Sesquiterpene β-caryophyllene Sesquiterpene α-humulene Sesquiterpene γ-muurolene Sesquiterpene Germacrene D [0.65] * Sesquiterpene β-selinene [0.65] * Sesquiterpene Bicyclogermacrene Sesquiterpene γ-cadinene Sesquiterpene δ-cadinene Sesquiterpene Caryophyllene oxide * Sesquiterp. ether Viridiflorol Sesquiterp. alcohol τ-cadinol Sesquiterp. alcohol Dimer of α-phellandrene II tr [0.12] * Diterpene Serratol Diterp. alcohol Total identified 99.02% 99.59% *: Two or more compounds are coeluting on this column [xx]: Duplicate percentage due to coelutions, not taken account in the identified total Note: no correction factor was applied OTHER DATA Physical aspect : Faintly yellow liquid Refractive index : ± (20 C) CONCLUSION No adulterant, contaminant or diluent were detected using this method. Page 3 of 5

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Alexis St-Gelais, M. Sc., chimiste

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