Filtration and Beverage Treatment Products. Fruit Juice & Fruit Wine Guide

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Filtration and Beverage Treatment Products Fruit Juice & Fruit Wine Guide

Fruit Juice Processing from Stone Fruit Process steps Production of concentrate from sour cherries (clear juice) Ripe and sound, fresh or frozen fruit Thawing of frozen fruit Mash heating to 140 158 F (60 70 C) Mechanical stone removal (if required) Crusher Enzyme dosage Mash heating Low pectin content eliminates mash and prevents instability of juices. Mash 1 2 h, 122 F (50 C) stir occasionally No mash maceration time. Continuously fill the press in order to prevent stones from settling in the mash tank. using a press or decanter (only mash from fruit without stones). For belt presses increase thickness of non-destoned mash. Centrifuge Aroma recovery Enzymation + fining Pectin degradation: approx. 1 2 h at 122 131 F (50 55 C) Panzym Pro Color enzyme: 0.61 1.53 fl oz/short ton (20 50 ml/t) or Panzym BE XXL enzyme: 0.46 0.92 fl oz/short ton (15 30 ml/t) Panzym Flux enzyme: 0.31 0.92 fl oz/shortton (10 30 ml/t) SIHA PURANIT TM / SIHA PURANIT UF fining agent: 15.34 30.68 oz/short ton (500 1,000 g/t) Gelatine Fine Granules fining agent: 1.53 3.07 oz/short ton (50 100 g/t) SIHA Pea Protein fining agent: 1.53 3.07 oz/short ton (50 100 g/t) SIHA Potato Protein fining agent: 0.76 1.53 oz/short ton (25 50 g/t) Lees filtration BECOLITE TM 5000 perlite Diatomaceous earth filtration Sheet filtration fine BECOGUR TM 200 diatomaceous earth (approx. 10%) BECO KD 10 or BECOPAD 350 depth filter sheets Storage tank Concentration with simultaneous sterile and polishing filtration of semi-concentrate (35 40 Brix) at 158 176 F (70 80 C) with BECO SD 30 or BECOPAD 270 depth filter sheets Flow: 0.20 gpm/ft² (500 l/m²/h) Concentration and sterile filtration BEVASIL is a registered trademark of Akzo Nobel GmbH 2

Production of concentrate from plums (clear juice) Ripe and sound, fresh or frozen fruit Thawing of frozen fruit Mash heating to 122 131 F (50 55 C) Mechanical stone removal (if required) Panzym Pro Color enzyme: 3.07 4.60 fl oz/short ton (100 150 ml/t) or Panzym BE XXL enzyme: 2.54 3.68 fl oz/short ton (80 120 ml/t) 1 2 h at 122 131 F (50 55 C) stir occasionally using a press or decanter (only mash from fruit without stones). For belt presses increase thickness of non-destoned mash. Pectin degradation: approx. 1 2 h at 122 131 F (50 55 C) Panzym Pro Color enzyme: 1.53 2.54 fl oz/short ton (50 80 ml/t) or Panzym BE XXL enzyme: 0.92 1.84 fl oz/short ton (30 60 ml/t) Panzym Flux enzyme: 0.31 0.92 fl oz/short ton (10 30 ml/t) SIHA PURANIT / SIHA PURANIT UF fining agent: 15.34 oz/short ton (500 g/t) Gelatine Fine Granules fining agent: 1.53 3.07 oz/short ton (50 100 g/t) SIHA Pea Protein fining agent: 1.53 3.07 oz/short ton (50 100 g/t) SIHA Potato Protein fining agent: 0.76 1.53 oz/short ton (25 50 g/t) BECOLITE 5000 perlite BECOGUR 200 diatomaceous earth (approx. 10%) BECO KD 10 or BECOPAD 350 depth filter sheets Concentration with simultaneous sterile and polishing filtration of semi-concentrate (35 40 Brix) at 158 176 F (70 80 C) with BECO SD 30 or BECOPAD 270 depth filter sheets Flow: 0.20 gpm/ft² (500 l/m²/h) 3

Fruit Juice Processing from Soft Fruit Process steps Production of concentrate from strawberries (clear juice) Ripe and sound, fresh or frozen fruit Thawing of frozen fruit Mash heating to 120 131 F (50 55 C) or cold enzyming at approx. 68 F (20 C) to protect the color Crusher Enzyme dosage Mash Mash heating 1 2 h, 122 F (50 C) stir occasionally Panzym Pro Color enzyme: 1.53 2.54 fl oz/short ton (50 80 ml/t) or Panzym BE XXL enzyme: 0.92 1.53 fl oz/short ton (30 50 ml/t) For frozen fruit, the dosages may have to be increased significantly. For cold enzyming, the dosages should be doubled. 1 2 h at 122 131 F (50 55 C) or 2 4 h at 68 F (20 C) stir occasionally using a press or decanter Centrifuge Aroma recovery Enzymation + fining Pectin degradation: approx. 1 2 h at 122 131 F (50 55 C) Panzym Pro Color enzyme: 0.61 1.53 fl oz/short ton (20 50 ml/t) or Panzym BE XXL enzyme: 0.46 0.92 fl oz/short ton (15 30 ml/t) Panzym Flux enzyme: 0.31 0.92 fl oz/short ton (10 30 ml/t) SIHA PURANIT / SIHA PURANIT UF fining agent: 15.34 oz/short ton (500 g/t) Gelatine Fine Granules fining agent: 1.53 3.07 oz/short ton (50 100 g/t) SIHA Pea Protein fining agent: 1.53 3.07 oz/short ton (50 100 g/t) SIHA Potato Protein fining agent: 0.76 1.53 oz/short ton (25 50 g/t) Lees filtration BECOLITE 5000 perlite BECOGUR 200 diatomaceous earth (approx. 10%) Diatomaceous earth filtration Sheet filtration fine Storage tank BECO KD 10 or BECOPAD 350 depth filter sheets Concentration with simultaneous sterile and polishing filtration of semi-concentrate (35 40 Brix) at 158 176 F (70 80 C) with BECO SD 30 or BECOPAD 270 depth filter sheets Flow: 0.20 gpm/ft² (500 l/m²/h) Concentration and sterile filtration BEVASIL is a registered trademark of Akzo Nobel GmbH 4

Production of concentrate from raspberries (clear juice) Ripe and sound, fresh or frozen fruit Thawing of frozen fruit Mash heating to 122 131 F (50 55 C) Panzym Pro Color enzyme: 1.84 3.68 fl oz/short ton (60 120 ml/t) or Panzym BE XXL enzyme: 1.53 3.07 fl oz/short ton (50 100 ml/t) For frozen fruit, the dosages may have to be increased significantly. 1 2 h at 122 131 F (50 55 C) stir occasionally using a press or decanter Pectin degradation: approx. 1 2 h at 122 131 F (50 55 C) Panzym Pro Color enzyme: 0.61 1.53 fl oz/short ton (20 50 ml/t) or Panzym BE XXL enzyme: 0.46 0.92 fl oz/short ton (15 30 ml/t) Panzym Flux enzyme: 0.31 0.92 fl oz/short ton (10 30 ml/t) SIHA PURANIT / SIHA PURANIT UF fining agent: 15.34 oz/short ton (500 g/t) Gelatine Fine Granules fining agent: 1.53 3.07 oz/short ton (50 100 g/t) SIHA Pea Protein fining agent: 1.53 3.07 oz/short ton (50 100 g/t) SIHA Potato Protein fining agent: 0.76 1.53 oz/short ton (25 50 g/t) BECOLITE 5000 perlite BECOGUR 200 diatomaceous earth (approx. 10%) BECO KD 10 or BECOPAD 350 depth filter sheets Concentration with simultaneous sterile and polishing filtration of semi-concentrate (35 40 Brix) at 158 176 F (70 80 C) with BECO SD 30 or BECOPAD 270 depth filter sheets Flow: 0.20 gpm/ft² (500 l/m²/h) 5

Fruit Juice Processing from Soft Fruit Process steps Production of concentrate from blackcurrants Ripe and sound, fresh or frozen fruit Thawing of frozen fruit Mash heating to 113 122 F (45 50 C) Crusher Enzyme dosage Mash heating Panzym Pro Color enzyme: 3.07 6.14 fl oz/short ton (100 200 ml/t) or Panzym BE XXL enzyme: 2.45 4.91 fl oz/short ton (80 160 ml/t) For frozen fruit, the dosages may have to be increased significantly. Mash 1 2 h, 122 F (50 C) stir occasionally 1 2 h at 113 122 F (45 50 C) stir occasionally using a press or decanter Centrifuge Aroma recovery Enzymation + fining Pectin degradation: approx. 1 2 h at 122 131 F (50 55 C) Panzym Pro Color enzyme: 0.92 1.84 fl oz/short ton (30 60 ml/t) or Panzym BE XXL enzyme: 0.61 1.23 fl oz/short ton (20 40 ml/t) Panzym Flux enzyme: 0.31 0.92 fl oz/short ton (10 30 ml/t) SIHA PURANIT/SIHA PURANIT UF fining agent: Gelatine Fine Granules fining agent: 3.07 6.14 oz/short ton (100 200 g/t) SIHA Pea Protein fining agent: 3.07 6.14 oz/short ton (100 200 g/t) SIHA Potato Protein fining agent: 1.53 3.07 oz/short ton (50 100 g/t) Lees filtration BECOLITE 5000 perlite Diatomaceous earth filtration Sheet filtration fine BECOGUR 200 diatomaceous earth (approx. 10%) BECO KD 10 or BECOPAD 350 depth filter sheets Storage tank Concentration with simultaneous sterile and polishing filtration of semi-concentrate (35 40 Brix) at 158 176 F (70 80 C) with BECO SD 30 or BECOPAD 270 depth filter sheets Flow: 0.20 gpm/ft² (500 l/m²/h) Concentration and sterile filtration BEVASIL is a registered trademark of Akzo Nobel GmbH 6

Production of concentrate from blackberries (clear juice) Ripe and sound, fresh or frozen fruit Thawing of frozen fruit Mash heating to 122 131 F (50 55 C) Panzym Pro Color enzyme: 2.45 4.91 fl oz/short ton (80 160 ml/t) or Panzym BE XXL enzyme: 1.84 3.68 fl oz/short ton (60 120 ml/t) For frozen fruit, the dosages may have to be increased significantly. 1 2 h at 122 131 F (50 55 C) stir occasionally using a press or decanter Pectin degradation: approx. 1 2 h at 122 131 F (50 55 C) Panzym Pro Color enzyme: 0.61 1.53 fl oz/short ton (20 50 ml/t) or Panzym BE XXL enzyme: 0.46 0.92 fl oz/short ton (15 30 ml/t) Panzym Flux enzyme: 0.31 0.92 fl oz/short ton (10 30 ml/t) SIHA PURANIT/SIHA PURANIT UF fining agent: Gelatine Fine Granules fining agent: 3.07 6.14 oz/short ton (100 200 g/t) SIHA Pea Protein fining agent: 3.07 6.14 oz/short ton (100 200 g/t) SIHA Potato Protein fining agent: 1.53 3.07 oz/short ton (50 100 g/t) BECOLITE 5000 perlite BECOGUR 200 diatomaceous earth (approx. 10%) BECO KD 10 or BECOPAD 350 depth filter sheets Concentration with simultaneous sterile and polishing filtration of semi-concentrate (35 40 Brix) at 158 176 F (70 80 C) with BECO SD 30 or BECOPAD 270 depth filter sheets Flow: 0.20 gpm/ft² (500 l/m²/h) 7

AJC and Fruit Juice Processing from Pomaceous Fruit Process steps Production of AJC with hot clarification + sterile filtration Ripe, sound, washed Crusher Enzyme dosage Mash Mash heating 0.5 1 h, 68 F (20 C) do not stir Panzym First Yield enzyme: 2.15 3.07 fl oz/short ton (70 100 ml/t) or Panzym YieldMASH XXL enzyme: 1.53 2.15 fl oz/short ton (50 70 ml/t) at approx. 68 F (20 C) without stirring Bucher press: 0.5 1 h Belt press: 1 h Decanter: 1 h Centrifuge Aroma recovery Enzymation + fining with possible secondary extraction pomace/water ratio = 1:0.5 1 Starch degradation: approx. 1 h at 122 131 F (50 55 C) Panzym HT 300 enzyme: 0.61 1.84 fl oz/short ton (20 60 ml/t) or Panzym AG XXL enzyme: 0.31 0.92 fl oz/short ton (10 30 ml/t) Check via iodine test Pectin degradation: approx. 1 h at 122 131 F (50 55 C) Panzym Pro Clear enzyme: 0.31 0.92 fl oz/short ton (10 30 ml/t) or Panzym XXL enzyme: 0.31 0.92 fl oz/short ton (10 30 ml/t) Panzym Flux enzyme: 0.31 0.92 fl oz/short ton (10 30 ml/t) SIHA PURANIT/SIHA PURANIT UF fining agent: 30.68 oz/short ton (1,000 g/t) Gelatine Fine Granules fining agent: 3.07 6.14 oz/short ton (100 200 g/t) SIHA Pea Protein fining agent: 3.07 6.14 oz/short ton (100 200 g/t) SIHA Potato Protein fining agent: 1.53 3.07 oz/short ton (50 100 g/t) Lees filtration Diatomaceous earth filtration Sheet filtration fine Storage tank BECOLITE 5000 perlite BECOGUR 200 diatomaceous earth (approx. 10%) BECO KDS 12 or BECOPAD 350 depth filter sheets Concentration with simultaneous sterile and polishing filtration of semi-concentrate (35 40 Brix) at 158 176 F (70 80 C) with BECO SD 30 or BECOPAD 270 depth filter sheets Flow: 0.20 gpm/ft² (500 l/m²/h) Concentration and sterile filtration BEVASIL is a registered trademark of Akzo Nobel GmbH 8

Production of clear apple juice with cold clarification Ripe, sound, washed Panzym First Yield enzyme: 2.15 3.07 fl oz/short ton (70 100 ml/t) or Panzym YieldMASH XXL enzyme: 1.53 2.15 fl oz/short ton (50 70 ml/t) at approx. 68 F (20 C) without stirring Bucher press: 0.5 1 h Belt press: 1 h Decanter: 1 h with possible secondary extraction pomace/water ratio = 1:0.5 1 Without previous aroma recovery Starch degradation: approx. 4 h at approx. 68 F (20 C) Panzym F2 enzyme: 1.53 4.60 fl oz/short ton (50 150 ml/t) Check via iodine test Pectin degradation: approx. 4 h at approx. 68 F (20 C) Panzym Pro Clear enzyme: 0.31 0.92 fl oz/short ton (10 30 ml/t) or Panzym XXL enzyme: 0.31 0.92 fl oz/short ton (10 30 ml/t) Panzym Flux enzyme: 0.31 0.92 fl oz/short ton (10 30 ml/t) SIHA PURANIT/SIHA PURANIT UF fining agent: Gelatine Fine Granules fining agent: 3.07 6.14 oz/short ton (100 200 g/t) SIHA Pea Protein fining agent: 3.07 6.14 oz/short ton (100 200 g/t) SIHA Potato Protein fining agent: 1.53 3.07 oz/short ton (50 100 g/t) BECOLITE 5000 perlite BECOGUR 200 diatomaceous earth (approx. 10%) BECO KDS 12 or BECOPAD 350 depth filter sheets Storage or bottling 9

2 nd Mash Enzymation and Fruit Juice Processing from Pomaceous Fruit Process steps Yield increase through 2 nd mash 1 part pomace from 1 st pressing + 0.6 1 part (depending on first yield from 60 80%) demineralized water at 176 194 F (80 90 C) Centrifuge Crusher Enzyme dosage Aroma recovery 2 nd Mash 2 h, 122 F (50 C) Stirring Mash heating Water 176 194 F (80 90 C) Lees filtration Enzymation + fining Diatomaceous earth filtration 1 st Mash 0.5 1 h, 68 F (20 C) do not stir Mash enzyme dosage, depending on first yield: Panyzm Second Yield enzyme a) 80% yield: 7.67 15.34 fl oz/short ton (250 500 ml/t) pomace b) 70% yield: 4.91 11.66 fl oz/short ton (160 380 ml/t) pomace c) 60% yield: 3.68 7.36 fl oz/short ton (120 240 ml/t) pomace 2. mash tenure: 122 131 F (50 55 C) with vigorous stirring using a press or decanter possibly followed by blending of 1 st juice and 2 nd juice Starch degradation: approx. 1 h at 122 131 F (50 55 C) Panzym HT 300 enzyme: 0.61 1.84 fl oz/short ton (20 60 ml/t) or Panzym AG XXL enzyme: 0.31 0.92 fl oz/short ton (10 30 ml/t) Check via iodine test Pectin degradation: approx. 1 h at 122 131 F (50 55 C) Panzym Pro Clear enzyme: 0.31 0.92 fl oz/short ton (10 30 ml/t) or Panzym XXL enzyme: 0.31 0.92 fl oz/short ton (10 30 ml/t) Panzym Flux enzyme: 0.31 0.92 fl oz/short ton (10 30 ml/t) SIHA PURANIT/SIHA PURANIT UF fining agent: 30.68 oz/short ton (1,000 g/t) Gelatine Fine Granules fining agent: 3.07 6.14 oz/short ton (100 200 g/t) SIHA Pea Protein fining agent: 3.07 6.14 oz/short ton (100 200 g/t) SIHA Potato Protein fining agent: 1.53 3.07 oz/short ton (50 100 g/t) BECOLITE 5000 perlite BECOGUR 200 diatomaceous earth (approx. 10%) Sheet filtration fine BECO KDS 12 or BECOPAD 350 depth filter sheets Storage tank Concentration with simultaneous sterile and polishing filtration of semi-concentrate (35 40 Brix) at 158 176 F (70 80 C) with BECO SD 30 or BECOPAD 270 depth filter sheets Flow: 0.20 gpm/ft² (500 l/m²/h) Concentration and sterile filtration 10 BEVASIL is a registered trademark of Akzo Nobel GmbH * Please refer to national law

Production of naturally cloudy apple juice Fully ripe (low starch content), sound and washed Panzym YieldMASH XXL enzyme: 0.92 1.53 fl oz/short ton (30 50 ml/t) Panzym First Yield enzyme: 1.23 1.84 fl oz/short ton (40 60 ml/t) 0.5 1 h at approx. 68 F (20 C) without stirring using a press or decanter Vitamin C dosage: 6.14 12.27 oz/short ton (200 400 g/t) * directly into the buffer tank Removal of instable solids via centrifuge Early pasteurization without long intermediate storage to prevent solid loss of stability through enzymatic activity and fermentation. Storage or filling: If no centrifuge was used for the removal of instable solids, the juice should be drawn off the coarse unfiltered sediment in the storage tank prior to bottling. 11

Fruit Juice Processing from Pomaceous, Pitted and Soft Fruit Small-scale fruit processors and fruit distilleries: Recommendations for processing of clear juices Process steps Pomaceous fruit (clear juice) Pomaceous fruit: apple, pear, quince Ripe, sound, washed and grinded fruits Crusher Enzyme dosage Mash 0.5 1 h, 68 F (20 C) do not stir Approx. 1 h at 68 F (20 C), without stirring Panzym Univers enzyme: 12.80 oz/1,000 gal (10 ml/hl) Pay attention to an even distribution of enzyme in the mash : Oxidation protection (as required): Ascorbic acid stabilizer: 1.67 3.34 lb/1,000 gal (20 40 g/hl) Juice : 2 4 h at 68 F (20 C): Starch degradation: Panzym F2 enzyme: 0.64 2.56 oz/1,000 gal (0.5 2 ml/hl) Pectin degradation: Panzym Univers enzyme: 1.28 2.56 oz/1,000 gal (1 2 ml/hl) Enzymation Diatomaceous earth filtration Lees filtration Fining: 6 8 h at 68 F (20 C): SIHA Active Bentonite G fining agent: approx. 8.35 lb/1,000 gal (100 g/hl) (at ph < 3.5 and 68 F (20 C) SIHA Ca-Bentonite G fining agent: approx. 8.35 lb/1,000 gal (100 g/hl)) BEVASIL 30 silica sol fining agent: 6.4 12.8 oz/1,000 gal (50 100 ml/hl) (higher dosing required for fruit rich in tannin) Gelatine Fine Granules fining agent: 0.83 2.5 lb/1,000 gal (10 30 g/hl) SIHA Pea Protein fining agent: 0.83 2.5 lb/100 gal (10 30 g/hl) SIHA Potato Protein fining agent: 0.42 xxx lb/100 gal (5 15 g/hl) Coarse filtration: BECOGUR 200 diatomaceous earth: approx. 10% at 0.84 1.67 lb/100 gal (100 200 g/hl) BECOGUR 3500 diatomaceous earth: approx. 90% at 0.84 1.67 lb/100 gal (100 200 g/hl) or BECOPAD 580 depth filter sheet Fine filtration: BECOPAD 350 depth filter sheet Storage tank Sheet filtration fine BECOLITE 5000 perlite: 102.24 143.42 lb/100 ft² (5 7 kg/m²) Bottling at approx. 176 F (80 C), depending on germ load and heat holding time BEVASIL is a registered trademark of Akzo Nobel GmbH 12

Pitted fruit/soft fruit (clear juice) Pitted fruit: cherry, plum, mirabelle plum Soft fruit: blackcurrant, strawberry, blackberry Ripe, sound, washed and grinded fruits 1 2 h at 113 131 F (45 55 C), occasional stirring Colored fruits: Panzym Univers enzyme: 0.83 2.5 lb/1,000 gal (10 30 g/hl) For cherry processing: Alternatively hot pressing at 140 158 F (60 70 C) without using enzymes : Juice : 2 4 h at 122 131 F (50 55 C) or 8 12 h at 68 F (20 C): Panzym Univers enzyme: 2.56 10.24 lb/1,000 gal (2 8 ml/hl) Fining: 1 2 h at 122 131 F (50 55 C) or 4 8 h at 68 86 F (20 30 C) SIHA Active Bentonite G fining agent: 2.09 4.17 lb/1,000 gal (25 50 g/hl) (at ph < 3.5 and 68 F (20 C) SIHA Ca-Bentonite G fining agent: approx. 2.09 4.17 lb/1,000 gal (25 50 g/hl)) BEVASIL 30 silica sol fining agent: 6.4 25.6 oz/100 gal (50 200 ml/hl) Gelatine Fine Granules fining agent: 0.42 1.67 lb/1,000 gal (5 20 g/hl) SIHA Pea Protein fining agent: 0.42 1.67 lb/100 gal (5 20 g/hl) SIHA Potato Protein fining agent: xxx 0.83 lb/100 gal (2.5 10 g/hl) Coarse filtration: BECOGUR 200 diatomaceous earth: approx. 10% at 0.84 1.67 lb/100 gal (100 200 g/hl) BECOGUR 3500 diatomaceous earth: approx. 90% at 0.84 1.67 lb/100 gal (100 200 g/hl) or BECOPAD 580 depth filter sheet Fine filtration: BECOPAD 350 depth filter sheet Colored juices: BECOPAD 450 depth filter sheet BECOLITE 5000 perlite: 102.24 143.42 lb/100 ft² (5 7 kg/m²) Bottling at approx. 176 F (80 C), depending on germ load and heat holding time 13

Fruit Wine Processing from Pomaceous, Pitted and Soft Fruit Process steps Crusher Enzyme dosage Enzymation Mash 0.5 1 h, 68 F (20 C) do not stir Fruit wine Pomaceous fruit: apple, pear quince pitted fruit: cherry, plum, mirabelle plum soft fruit: blackcurrant, strawberry, blackberry Ripe, sound, washed and grinded fruit Pomaceous fruit: approx. 1 h at 68 F (20 C) without stirring, Panzym Univers enzyme: 12.80 oz/1,000 gal (10 ml/hl) Pitted/soft fruit: 1 2 h at 113 131 F( 45 55 C), occasional stirring Rich-colored fruit: Panzym Univers enzyme: 12.80 38.4 oz/1,000 gal (10 30 ml/hl) : Juice stabilization: Addition of sulfur: SIHA Potassium Pyrosulphite stabilizer: 0.5 0.83 lb/1,000 gal (6 10 g/hl) Addition should follow the microbiological burden of incoming fruit Juice : Starch degradation (pomaceous fruit): Panzym F2 enzyme: 0.64 2.56 oz/1,000 gal (0.5 2 ml/hl) Pectin degradation: Panzym Univers enzyme: 0.64 2.56 oz/1,000 gal (0.5 2 ml/hl) No holding time: Starch and pectin degradation occur during fermentation Chaptalization (as required) Acification: Lactic Acid 80% stabilizer: max. 3.13 lb/100 gal (3.75 g/l)* (optional for fruits low in acid) Fermentation (make sure to only use cleaned fermentation vessels with fermentation air locks): SIHA Active Yeast 3: 1.67 lb/1,000 gal (20 g/hl) SIHA Active Yeast 8 (Burgundy Yeast): 1.67 lb/1,000 gal (20 g/hl) Rehydration of active dry yeast in juice water mixture (50:50) with SIHA SpeedFerm yeast nutrient Yeast nutrient: Fermentation Salt yeast nutrient: max. 2.5 lb/1,000 gal (30 g/hl), step-wise addition until mid of fermentation Fermentation temperature: 60.8 64.4 F (16 18 C) After fermentation: Racking followed by sulfurization with 1 1.34 lb/1,000 gal (12 16 g/hl) SIHA Potassium Pyrosulphite stabilizer Fining: SIHA Active Bentonite G fining agent: approx. 2.09 8.35 lb/1,000 gal (25 100 g/hl) (at ph < 3.5 SIHA Ca-Bentonite G fining agent: approx. 8.35 lb/1,000 gal (100 g/hl)) BEVASIL 30 silica sol fining agent: 6.4 25.6 oz/1,000 gal (50 200 ml/hl) (higher dosing required for fruit rich in tannin) Gelatine Fine Granules fining agent: 0.83 1.67 lb/1,000 gal (5 20 g/hl) SIHA Pea Protein fining agent: 0.42 1.67 lb/100 gal (5 20 g/hl) SIHA Potato Protein fining agent: 0.02 0.83 lb/100 gal (2.5 10 g/hl) 14 Diatomaceous earth filtration Storage tank Lees filtration Sheet filtration fine Stabilitzation: SIHA Potassium Pyrosulphite stabilizer: target value, free SO 2 : 0.05 0.07 oz/1,000 gal (35 50 mg/l) Potassium Sorbate stabilizer: max. 2.24 lb/1,000 gal (26.8 g/hl) (for wines with residual sugar) Coarse filtration: BECOGUR 200 diatomaceous earth: approx. 10% at 0.84 1.67 lb/100 gal (100 200 g/hl) BECOGUR 3500 diatomaceous earth: approx. 90% at 0.84 1.67 lb/100 gal (100 200 g/hl) or BECOPAD 580 depth filter sheet Fine filtration: BECOPAD 350 depth filter sheet Sterile filtration: BECOPAD 220 depth filter sheet BECOLITE 5000 perlite: 102.24 143.42 lb/100 ft² (5 7 kg/m²) * Guidelines from March 1, 2003 BEVASIL is a registered trademark of Akzo Nobel GmbH

Fruit Wine Processing from Apples and Pears (Cider) Process steps Cider Ripe, sound and washed fruit Crusher Enzyme dosage Mash heating First mash dosage: Panzym First Yield enzyme: 2.15 3.07 fl oz/short ton (70 100 ml/t) Second mash 2 h, 122 F (50 C) stir Water 176 194 F (80 90 C) First mash 0.5 1 h, 68 F (20 C) do not stir First mash : At approx. 68 F (20 C), without stirring Possible process step: juice extraction with secondary extraction (second mash ): Maximum yield, Panzym Second Yield enzyme: 3.07 6.14 fl oz/short ton (100 200 ml/t) pomaceous fruit 1.5 2 h at 122 131 F (50 55 C), with vigorous stirring : Possibly blending of first and second juice Centrifuge Alcoholic fermentation: SIHA Active Yeast 3 or SIHA Active Yeast 8 (Burgundy Yeast): 1.67 lb/100 gal (20 g/hl) Rehydration of active dry yeast in juice water mixture (50:50) at 95 F (35 C) Fermentation temperature: 63 72 F (17 22 C) Enzymation/alcoholic fermentation: Panzym Flux enzyme: 0.31 0.92 fl oz/short ton (10 30 ml/t) for pectin degradation and improved sedimentation Higher alcohol yield with Panzym HT 300 enzyme: 0.61 0.92 fl oz/short ton (20 30 ml/t) Rehydration of active dry yeast: SIHA SpeedFerm yeast nutrient: 1.67 lb/100 gal (20 g/hl) Fermentation Yeast nutrients: Fermentation Salt yeast nutrient: max. 0.84 lb/100 gal (100 g/hl), step-wise addition until mid of alcoholic fermentation SIHA Vitamin B 1 yeast nutrient: max. 0.005 lb/1,000 gal (0.6 g/1000 l) SIHA PROFERM H+ 2 combined yeast nutrient: max. 3.3 lb/1,000 gal (40 g/hl) Optional: malolactic fermentation (MLF): SIHALACT Oeno lactic acid bacteria (citrate-positive) after alcoholic fermentation Diatomaceous earth filtration Sediment filtration Diatomaceous earth filtration: BECOGUR 200 diatomaceous earth: approx. 10% at 0.84 1.67 lb/100 gal (100 200 g/hl) BECOGUR 3500 diatomaceous earth: approx. 90% at 0.84 1.67 lb/100 gal (100 200 g/hl) Stabilization: Cold stabilization: BECO Steril 40 or BECO KDS 15 depth filter sheets Room temperature: BECOPAD 220, BECO KD 10 or BECO Steril 40 depth filter sheets Storage tank Sheet filtration fine 15

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