Quality of western Canadian flaxseed 2014

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ISSN 1700-2087 Quality of western Canadian flaxseed 2014 Ann S. Puvirajah Oilseeds Contact: Ann S. Puvirajah Oilseeds Tel : 204 983-3354 Email: ann.puvirajah@grainscanada.gc.ca Fax : 204-983-0724 Grain Research Laboratory Canadian Grain Commission 1404-303 Main Street Winnipeg MB R3C 3G8 www.grainscanada.gc.ca Quality Innovation Service

Table of contents Introduction... 4 Summary... 5 Weather and production review... 6 Weather review, seeding and growing conditions... 6 Production and grade information... 6 Harvest samples... 7 Quality data by province and western Canada... 8 Oil content... 10 Protein content... 11 Free fatty acids content... 12 Fatty acid composition... 13 Tables Table 1 Flaxseed, No. 1 Canada Western Quality data for 2014 harvest... 5 Table 2 Flaxseed, No. 1 Canada Western Fatty acid composition for 2014 harvest... 5 Table 3 Seeded area and production for western Canadian flaxseed... 7 Table 4 Flaxseed, No. 1 Canada Western Quality data for 2014 harvest... 9 Table 5 Flaxseed, No. 1 Canada Western Fatty acid composition and free fatty acids content for 2014 harvest... 9 Figures Figure 1 Map of Prairie provinces showing traditional growing areas for flaxseed... 4 Figure 2 - Flaxseed, No. 1 Canada Western Oil content of harvest samples, 2004 2014... 10 Figure 3 - Flaxseed, No. 1 Canada Western Protein content of harvest samples, 2004 2014... 11 Figure 4 - Flaxseed, No. 1 Canada Western Free fatty acids content of harvest samples, 2004 2014... 12 Figure 5 Flaxseed, No. 1 Canada Western Linolenic acid content of harvest samples, 2004 2014... 14 Canadian Grain Commission 2 Quality of western Canadian flaxseed 2014

Figure 6 Flaxseed, No. 1 Canada Western Iodine value of harvest samples, 2004 2014... 14 Canadian Grain Commission 3 Quality of western Canadian flaxseed 2014

Introduction This report presents quality data and information based on samples of western Canadian flaxseed from the Canadian Grain Commission s 2014 Harvest Sample Program. The quality data includes oil, protein, free fatty acids, fatty acid composition and iodine values of harvest samples submitted to the Grain Research Laboratory. Producers and grain companies submitted the samples throughout the harvest period. The map shows the Prairie provinces, the traditional growing areas for flaxseed in western Canada.. Figure 1 Map of Prairie provinces showing traditional growing areas for flaxseed Source: Flax Council of Canada Canadian Grain Commission 4 Quality of western Canadian flaxseed 2014

Summary The Canadian Grain Commission s Harvest Sample Program of western Canadian flaxseed shows that the 2014 crop contains lower oil content, similar protein content and higher iodine values when compared to the 2013 harvest. Table 1 shows data for Flaxseed, No. 1 Canada Western. Oil content is 45.6%, 0.3% lower than the 2013 mean (45.9%) and similar to the 10-year mean (45.6%). Protein content is 21.1% and is slightly lower than the 2013 mean (21.2%) and 1.3% lower than the 10-year mean (22.4%). Iodine value is 192.9 units, which is 3.2 units higher than the 2013 value of 189.7 units. Environmental factors can play an important role in oil and protein content trends, as well as fatty acid composition. The Grain Research Laboratory s long-term harvest sample results have shown cool, wet growing conditions tend to produce a flaxseed crop with higher oil content and iodine values and lower protein content.. Table 1 - Flaxseed, No. 1 Canada Western Quality data for 2014 harvest Quality parameter 2014 2013 2004-2013 Mean Oil content 1, % 45.6 45.9 45.6 Protein content 2, % 21.1 21.2 22.4 Free fatty acids, % 0.2 0.1 0.2 Iodine value 192.9 189.7 191.5 1 Dry matter basis 2 N x 6.25; Dry matter moisture basis Table 2 - Flaxseed, No. 1 Canada Western Fatty acid composition for 2014 harvest Fatty acid 1, % in oil 2014 2013 2004-2013 Mean Palmitic acid (C16:0) 5.1 5.2 5.0 Stearic acid (C18:0) 3.2 3.3 3.3 Oleic acid (C18:1) 18.2 19.5 18.1 Linoleic acid (C18:2) 14.8 15.1 15.7 α-linolenic acid(c18:3) 57.9 56.0 57.0 1 Percentage of total fatty acids in the oil including palmitic (C16:0), stearic (C18:0), oleic (C18:1), linoleic (C18:2), and linolenic (C18:3) Canadian Grain Commission 5 Quality of western Canadian flaxseed 2014

Weather and production review Weather review, seeding and growing conditions The climate across the Prairies was quite varied throughout the 2014 growing season. April temperatures were 4 to 5 degrees lower than average, which delayed seeding for about 2 to 3 weeks. The majority of seeding was complete by early June. Precipitation also drastically increased in June, and there was localized flooding in some of the important flax growing regions such as southwestern Manitoba and southeastern Saskatchewan. While Manitoba and Saskatchewan received a lot of precipitation, some areas in Alberta had drought-like conditions. Harvest was also delayed due to excess moisture. The majority of the harvest was completed by the 3rd week of October. Source: http://www.agr.gc.ca Production and grade information Western Canadian farmers seeded 628,000 hectares of flaxseed in 2014 (Table 3), which is an increase compared to 2013 (418,000 hectares). The 2014 yield estimate of 1,400 kilograms per hectare was lower than the yield reported in 2013 (1,700 kilograms per hectare) and higher than the 10-year mean of 1,323 kilograms per hectare. Western Canada flaxseed production increased by134,000 metric tonnes from last year s 712,000 thousand metric tonnes. In Manitoba, production decreased to 53,000 metric tonnes, but increased in Saskatchewan to 706,000 metric tonnes and in Alberta to 87,000 metric tonnes when compared to 2013 production values. (Statistics Canada) Saskatchewan accounted for 84% of flaxseed production while Manitoba and Alberta had 6% and 10%, respectively. Over 98% of the samples received for the Canadian Grain Commission s 2014 Harvest Sample Program were graded as Flaxseed, No.1 Canada Western. Canadian Grain Commission 6 Quality of western Canadian flaxseed 2014

Table 3 - Seeded area and production for western Canadian flaxseed 1 Seeded area Production Average production 2014 2013 2014 2013 2004-2013 thousand hectares thousand tonnes thousand tonnes Manitoba 36 34 53 54 118 Saskatchewan 546 348 706 584 510 Alberta 46 36 87 74 40 Western Canada 628 418 846 712 668 1 Source: Statistics Canada. Table 001-0010 - Estimated areas, yield, production and average farm price of principal field crops, in metric units, annual, CANSIM (database). http://www5.statcan.gc.ca010010& Harvest samples Flaxseed samples for the Canadian Grain Commission s Harvest Sample Program are collected and cleaned to remove dockage prior to testing. The samples are analyzed for oil, protein and iodine value using a Foss NIRSystems 6500 scanning near-infrared spectrometer, calibrated to and verified against the appropriate reference method. Composite samples are used for free fatty acids and fatty acid composition analyses. Composites are prepared by combining samples by province for Flaxseed, No.1 Canada Western. Composites of Flaxseed, No. 2 Canada Western, Flaxseed, No. 3 Canada Western and Sample Grade combine all samples from western Canada by grade. This year's harvest report includes 259 samples compared to 176 in 2013. Manitoba contributed 39 samples of Flaxseed, No. 1 Canada Western, Saskatchewan 180 samples, and Alberta 40 samples during the harvest period from September 1st to December 1st, 2014. Weighting factors are used to calculate provincial and western Canadian means. Canadian Grain Commission 7 Quality of western Canadian flaxseed 2014

Quality data by province and western Canada Tables 4 and 5 show detailed information on the quality of top grade western Canadian (CW) flaxseed harvested in 2014. Of the flaxseed samples submitted to the Grain Research Laboratory, 98% were graded as No. 1 Canada Western with the remaining 2% consisting of No. 2 Canada Western, No. 3 Canada Western and Sample grade. The number of harvest samples collected from each province may not represent the actual production or grade distribution. However, there were sufficient samples to provide good quality information for each province. To calculate western Canadian averages, provincial averages are weighted by the Statistics Canada production estimate and an estimate of grade distribution. Oil and protein content give quantitative estimates of the value of the seed as a source of oil and of the resulting meal as a source of protein for animal feed. Alphalinolenic acid is an omega-3 fatty acid which literature has shown can play an important role in maintaining good health in humans and animals (www.flaxcouncil.ca). It is the main factor in the increased use of whole and ground flaxseed in cereals and baked goods, and flaxseed oil in salads. Flaxseed is also used in animal feeds, for example in chicken to produce omega-3 eggs. Iodine value is a measure of the overall unsaturation of the oil and can be calculated from the fatty acid composition. Oils with higher iodine values, i.e., with more unsaturation, polymerize more rapidly in the presence of air. In flaxseed, iodine value is directly related to the amount of alpha-linolenic acid present in the oil. Alphlinolenic acid is one of the most important quality factors for industrial use as it is responsible for most of flaxseed oil s drying properties. Canadian Grain Commission 8 Quality of western Canadian flaxseed 2014

Table 4 - Flaxseed, No. 1 Canada Western Quality data for 2014 harvest Province Number of samples tested Oil content 1, % Protein content 2, % Iodine value Mean Min. Max. Mean Min. Max. Mean Min. Max. Manitoba 39 46.3 43.5 48.4 21.3 17.8 24.5 193.9 185.7 208.3 Saskatchewan 180 45.4 40.8 49.5 20.5 17.5 24.5 193.0 180.2 205.8 Alberta 40 45.7 41.7 50.1 23.5 19.1 26.4 191.0 182.5 201.7 Western Canada 3 259 45.6 40.8 50.1 21.1 17.5 26.4 192.9 180.2 208.3 1 Dry matter basis 2 N x 6,25; dry matter basis 3 Mean values are weighted averages based on estimated production by province (Statistics Canada). Table 5 Flaxseed, No. 1 Canada Western Fatty acid composition and free fatty acids content of 2014 harvest Province Fatty acid composition, % 1 Number of samples C16:0 C18:0 C18:1 C18:2 C18:3 Free fatty acids Manitoba 39 4.9 3.3 17.3 15.4 58.2 0.2 Saskatchewan 180 5.1 3.1 18.2 14.6 58.0 0.1 Alberta 40 5.1 3.4 18.9 14.9 56.8 0.2 Western Canada 2 259 5.1 3.2 18.2 14.8 57.9 0.2 1 Percentage of total fatty acids in the oil including palmitic (C16:0), stearic (C18:0), oleic (C18:1), linoleic (C18:2), and linolenic (C18:3) 2 Mean values are weighted averages based on estimated production by province (Statistics Canada). Canadian Grain Commission 9 Quality of western Canadian flaxseed 2014

Oil content Average oil content (45.6%) in Flaxseed. No. 1 Canada Western is similar to the 2013 average (45.9%) and is identical to the 10-year mean (45.6%) (Figure 2). Average oil content for Manitoba (46.3%) is higher than the average in Saskatchewan (45.4%) and Alberta (45.7%) (Table 4). Oil content for Flaxseed, No. 1 Canada Western samples from producers across western Canada ranged from 40.8 to 50.1% (Table 4). Figure 2 Flaxseed, No. 1 Canada Western Oil content of harvest samples, 2004-2014 46.5 Oil content (%, dry basis) 46 45.5 45 44.5 44 43.5 2004 2006 2008 2010 2012 2014 Year 2014 average... 45.6% 2013 average... 45.9% 2004 2013 mean... 45.6% Canadian Grain Commission 10 Quality of western Canadian flaxseed 2014

Protein content Average protein content (21.1%) for Flaxseed, No.1 Canada Western is similar to the 2013 harvest average (21.2%) and lower than the 10-year mean (22.4%) (Figure 3). The average in Manitoba (21.3%) is higher than the average in Saskatchewan (20.5%) and lower than the average in Alberta (23.5%). Protein content for Flaxseed, No. 1 Canada Western samples from producers across western Canada ranged from 17.5 to 26.4% (Table 4). Figure 3 Flaxseed, No. 1 Canada Western Protein content of harvest samples, 2004 2014 28.0 Protein content (%, dry baisis) 26.0 24.0 22.0 20.0 2004 2006 2008 2010 2012 2014 Year 2014 average... 21.1% 2013 average... 21.2% 2004 2013 mean... 22.4% Canadian Grain Commission 11 Quality of western Canadian flaxseed 2014

Free fatty acids content Average free fatty acids content (0.20%) in Flaxseed, No. 1 Canada Western is higher than the average in 2013 (0.13%) and the same as the 10-year mean (0.20) (Figure 4). The average in Manitoba (0.20%) is higher than the average in Saskatchewan (0.10%) and similar to the Alberta average (0.20%) (Table 5). Higher values are mainly due to seed damage. Samples that graded No. 2 Canada Western, No. 3 Canada Western and Sample grade all have an average free fatty acids content of 1.05%. Figure 4 Flaxseed, No. 1 Canada Western Free fatty acids content of harvest samples, 2004 2014 _ Free fatty acids content in oil (FFA, %) 0.40 0.20 0.00 2004 2006 2008 2010 2012 2014 Year 2014 average... 0.20% 2013 average... 0.13% 2004 2013 mean... 0.20% Canadian Grain Commission 12 Quality of western Canadian flaxseed 2014

Fatty acid composition Average alpha-linolenic acid (C18:3) content (57.9%) in Flaxseed, No. 1 Canada Western is higher than the average in 2013 (56.0%) and the 10-year mean (57.0%) (Figure 5). Values in samples of Flaxseed, No. 1 Canada Western from producers across western Canada ranged from 49.6% to 65.6%. The average iodine value of the oil from Flaxseed, No.1 Canada Western samples is 192.9 units. Iodine value is a measure of the total degree of unsaturation of the oil and, in flaxseed, is heavily influenced by the linolenic acid content of the oil. The 2014 iodine value is 3.2 units higher than in 2013 and 1.4 units higher than the 10- year mean of 191.5 units (Figure 6). Iodine values for Flaxseed, No.1 Canada Western samples from producers across western Canada varied from 180 to 208 units. Usually oils with iodine values greater than 188 units are desired by the coatings industry for products such as paints, varnishes and inks, while oils with iodine values around 183 units are preferred by the linoleum industry. Iodine value, like oil content, is influenced by growing temperatures and length of photoperiod.. Figure 5 Flaxseed, No. 1 Canada Western Canadian Grain Commission 13 Quality of western Canadian flaxseed 2014

Percent α Linolenic acid content of harvest samples, 2004 2014 62.0 α-linolenic acid in oil (%) in oil 60.0 58.0 56.0 54.0 52.0 50.0 2004 2006 2008 2010 2012 2014 Year 2014 average... 57.9% 2013 average... 56.0% 2004 2013mean... 57.0% Figure 6 Flaxseed, No. 1 Canada Western Iodine value of harvest samples, 2004 2014 Iodine value (units) 205.0 200.0 195.0 190.0 185.0 180.0 175.0 170.0 2004 2006 2008 2010 2012 2014 Year 2014 average... 192.9 2013 average... 189.7 2004 2013 mean... 191.5 Canadian Grain Commission 14 Quality of western Canadian flaxseed 2014