Dr. Ilona Schneider. Filter Practices that Protect Aroma Profile. Increasing Colour and Stability of Pinot Noir

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Filter Practices that Protect Aroma Profile Increasing Colour and Stability of Pinot Noir Aspects of Grape and Oenology Technology on Aromatic Whites Sparkling Blanc de Noir Production Dr. Ilona Schneider 2010 Eaton Corporation. All rights reserved.

History of wine style Sensory variation 1960`s 1970`s 1980`s 1990`s 2000`s 2010`s Off flavor, residual sugar Botrytis Juice clarification, whole cluster pressing, active dry yeast cold fermentation Barrique Terroir, spontaneous fermentation Nature wine Design wine authentic wine 2 2

Enology trends view from europe Spontaneous alcoholic fermentation Favorite exotic aroma Thiole-Aficionados Moderate alcohol Long yeast contact time Biotechnology (microorganisms, enzymes) instead of mechanical processing Lower oak influence in red - and white wine High volume barriques for white wines Wines from Amphore Production of individual signature wines 3 3

Trend: Wine style Easy-drinking: cold fermentation aroma fresh- fruity Expression of green exotic Sauvignon blanc Mineral driven, structured Terroir wine Complex, creamy Sponti Type Intensive Bouquet Wine (Aromatic wine) Rosé easy to drink Lifestyle Premium red wines without an overloading of tannins 4 4

Easy-drinking cold fermentation fresh - fruity Sugar concentration juice 70 80 Oe 7 9 g/l juice acidity Max. 10% Botrytis 30-50 mg/l SO 2, depending on ph Enzymation of juice, Bentonite finning Intensive juice clarification 10 30 NTU Yeast with high ester production (SIHA Cryarome, SIHA WhiteArome, SIHAFERM Element) Fermentation at beginning 15 C, stop cooling process depending on the fermentation speed of the yeast High demand of yeast nutrient (DAP, SIHA SpeedFerm) SO 2 -Addition 14 days after fermentation, no MLF, early racking. If residual sugar: stop fermentation of by cuve Early bottling: from nov. until spring Ronald Searle Winespeak, 1983 ronaldsearle.blogspot.com 5 5

Sensorical profile of long yeast sediment storage in 2009 Pinot Blanc (N = 16 person x 3 reputation) bitter Intensity* adstringency bitter Persistency* citrus** 6 5 4 3 2 1 0 control peach / apricot yeast * 8 month flowery green gras Acidity sweet honney** butter/yeasty*** significance: p <0,05; **p<0,01; ***p<0,001 M. Sokolowsky, U. Fischer 6 AiF FV 16006 6

International style of Sauvignon blanc (Fischer, Weinwelt 2011) Green note South Africa New Zealand Rasberry South Africa New Zealand France Chile, US, Austr. Chile, USA, Austr. France Fruit (passionfruit, citrus) Minerale 7 7

Expression of green exotic Sauvignon blanc Juice sugar concentration 80 90 Oe 7 10 g/l juice acdity No botrytis 1/3 early harvest (Pyrazine) 2/3 late harvest (Exotic) 50 mg/l SO 2 + 100 mg/l ascorbic acid Enzymation of juice, bentonite finning Intensive juice clarification 10 30 NTU Sauvignon Blanc yeast (SIHA Cryarome) Fermentation at beginning 16-18 C, stop cooling process depending on the fermentation speed of the yeast SO 2 Addition 14 days after fermentation, no MLF, racking 14 days before bottling, DE-Filtration No or low residual sugar O 2 -reduction bottling from feb., screw caps Ronald Searle Winespeak, 1983 ronaldsearle.blogspot.com 8 8

Trial 2010 Sauvignon Blanc Direct processing (DV) Mash treatment (MS) Trial set up DV 10 NTU DV 100 NTU DV 200 NTU MS 10 10 NTU MS 100 NTU MS 200 NTU MLF Bachelor M. Schneider FH Rhein-Main, FB Geisenheim, Co- inoc. MLF1 Co- inoc. MLF2 Co- inoc. MLF3 deacidification A Rosenberger, H.-G. Schmarr, DLR Rheinpfalz 9 9

Extraction of Isobutyl-Methoxypyrazine during mash treatment and press fraction 3,2 ng/l MS 0h MS 6h MS 10h Free run pressing Bachelor M. Schneider FH Rhein-Main, FB Geisenheim, A Rosenberger, H.-G. Schmarr, DLR Rheinpfalz 10 10

Isobutyl-Methoxypyrazine after bottling Difference 1,1 ng/l not relevant MS 10 NTU MS 100 NTU MS 200 NTU DV 10 NTU DV 100 NTU DV 200 NTU Bachelor M. Schneider FH Rhein-Main, FB Geisenheim, A Rosenberger, H.-G. Schmarr, DLR Rheinpfalz 11 11

5-point-scheme (n= 16) Validation DV 10 NTU DV 200 NTU DV 100 NTU MS 10 NTU MS 100 NTU MS 200 NTU Bachelor M. Schneider FH Rhein-Main, FB Geisenheim, A Rosenberger, H.-G. Schmarr, DLR Rheinpfalz 12 12

Optimale ripening of grapes Terroir unripen ripe overripen, botrytis Botrytis mask Terroir 70 80 90 100 110 Oe Sugar concentration 13 13

Complex, creamy Sponti Type Ronald Searle Winespeak, 1983 ronaldsearle.blogspot.com Sugar concentration 85 105 Oe, 6 10 g/l juice acidity Max. fresh 10% botrytis mashing (4 12h) with enzyme Moderate juice clairification 40-100 NTU no SO 2 spontaneous fill up the tank Fermentation and storage in big wood barrels Wait until fermentation starts Addition of nutrients like SIHA SpeedFerm, later SIHA Proferm Plus Fermentation temperature 20 C after ½ of fermentation addition of SIHAFERM Element SO 2 -Addition14 days after fermentation, no MLF, racking 14 days before bottling with DE-Filtration Natural residual sugar Sufficient SO 2 for a long bottle storage 14 14

Fermentation rate 96 86 76 Sugar concentration [ Oe] 66 56 46 36 26 16 6-4 1 8 15 22 29 36 43 50 Days [d] Spontaneous - Imitate Imitierte Spontangärung Virtuelle Spontaneous Spontangärung - virtual Klassische Spontaneous Spontangärung - classical Kontrolle control Reinzuchthefe Pied de Cuve Pied de cuve 15 15

Descriptive analysis (N = 21 persons) Spontaneous - classical Spontaneous - virtual control 16 16

Intensive Bouquet Wine Sugar concentration 90 115 Oe 6 9 g/l juice acidity only ripe, dried botrytis up to 30% 50 mg/l SO 2, alternative 100 mg/l Lysozyme Mash treatment with enzyme; active carbon in juice Filtration up to 10 50 NTU Yeast with high aroma precursor (SIHA 7) Fermentation to begin 18 C, fermentation cooling depending on fermentation rate SO 2 -Addition after fermentation, no MLF, early racking Favorable Residual sugar Sufficient free SO 2 for long storage Ronald Searle Winespeak, 1992 ronaldsearle.blogspot.com 17 17

Sensory profile grape processing 2009 Gewürztraminer (n = 18 P. x 3 R) bitter Persistency n.s. bitter Intensity n.s. astringent color <0,0001*** 6 5 4 3 2 1 0 citrus 0,007** peach <0,0001*** flowery <0,0001*** acidity 0,0266* honey <0,0001*** sweet 0,0134* butter/yeasty n.s. green grass n.s. control ph 3,6 Ac 5,1 whole cluster pressing, ph 3,4 Ac 5,8 mashing 8 h, ph 3,8 Ac 4,8 mashing 24 h, ph 3,9 Ac 4,5 18 18

Mashing Gewürztraminer 8 h holding time 70 60 50 sweet N= 12 x 3 Dominant rat rate [%] 40 30 20 sauer bitter alcoholic significant level coincident 10 adstringent 0 0 10 20 30 40 50 time [sec] 19 19

Mashing Gewürztraminer 24 h holding time 70 60 süß sweet N= 12 x 3 Dominanzrate [%] Diminant rate [%] 50 40 30 20 alkoholisch alcoholic bitter Significant Signifikanzlevel Coincident Zufallswahrscheinlichkeit 10 0 sauer adstringieren adstringent d 0 10 20 30 40 50 Time Zeit [sec.] [sec] 20 20

Rosé easy to drink Lifestyle Sugar concentration 65 85 Oe, 6 7 g/l juice acidity Destemming without crushing or whole cluster pressing Reduction of juice / Saignée process for red wines Juice enzymation, bentonite fining, as far there is botrytis grapes active carbon fining Clarification 10 30 NTU (Flotation N 2 ) Cold fermentation yeast (SIHA Cryarome, SIHA WhiteArome) Fermentation at the beginning 16 C, cooling down depending on fermentation rate High demand on yeast nutrient (Fermentation salt, SIHA SpeedFerm, SIHA Proferm H+2) SO 2 - Addition 14 days after fermentation, no MLF, fast racking. Colour adjustment by red wine Ronald Searle Winespeak, 1992 ronaldsearle.blogspot.com 21 21

Premium red wines without an overloading of tannins Sugar concentration 90 105 Oe 6 8 g/l juice acidity Destemming with crushing of 50% of berries 50 mg/l SO 2 Cold maceration 5 days at < 10 C Inocculation with yeast with positive Effect on polymerisation (Siha 10 Red Roman, SIHA Rubino Cru) 5 8 days fermentation at 30 C MLF, also co-inccoluation with high cell count 30 mg/l SO 2 before storage in barrique Bottling before harvest of the following year Ronald Searle Winespeak, 1992 ronaldsearle.blogspot.com 22 22

Cold maceration of 2011, Pinot Noir (B.Sc. Arbeit David Golitko, WeinCampus Neustadt) Sample Description 5+5 days 5 days cold maceration 5 days fermentation/maceration 5+10 days 5 days cold maceration 10 days fermentation/maceration 10 days 10 days fermentation/maceration 15 days 15 days fermentation/maceration vintage 2011 Auer 2107t Harvest: 15. Sept Maceration and fermentation 50 L tanks (15 L juice/ 35 kg grapes) n = 2 Cold maceration: 5 C Yeast: SIHA 10 50 mg/l SO 2 23 23

Influence of cold maceration on the sensory profile of pinot noir 2011 (B.Sc. Arbeit David Golitko) colour intensity*** 8 Colour Tone *** Bitter NS 7 (brown --> violet) 6 Astringent * 5 strawberry * 4 3 2 dry tannins** 1 dry fruit NS 0 green tannins NS mouthfeel * (hart --> soft) medicine ** spicy NS Mint * cherry NS 5+5 days 5+10 days 10 days 15 days 24 24

Influence of colour intensity on pinot noir 2011 (B.Sc. Arbeit David Golitko) 6 5 colour intensity [AU] 4 3 2 1 0 Cold maceration 3x more anthocyane at fermentation begin 5+5 days 5+10 days 10 days 15 days days in relation to fermenation begin Cold maceration 25 25

Extraction of phenol on pinot noir 2011 (B.Sc. Arbeit David Golitko, WeinCampus Neustadt) 140 Flavan-3-ol monomere [mg/l] 120 100 80 60 40 20 5+5 days 5+10 days 10 days 15 days 0 Cold maceration days in relation to fermentation begin 26 26

Influence of maceration on ratio Flavanol Anthocyane MOX negative MOX positive MOX positive MOX without any effect Durner et al, 2010, AJEV 27 27

Model of Sensory data (B.Sc. Arbeit David Golitko, WeinCampus Neustadt) 28 28

Filter Practices that Protect Aroma Profile Increasing Colour and Stability of Pinot Noir Aspects of Grape and Oenology Technology on Aromatic Whites Sparkling Blanc de Noir Production Dr. Ilona Schneider 2010 Eaton Corporation. All rights reserved.