Consumables and Spare Parts Catalog TS 4000 Analzyer Version: 1.0.0

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Consumables and Spare Parts Catalog TS 4000 Analzyer Version: 1.0.0 Figure 1 1. TS 4000 analyzer Thermo Fisher Scientific Consumables & Spare/Service Parts Catalog i

Disclaimer Technical information contained in this publication is for reference purposes only and is subject to change without notice. Every effort has been made to supply complete and accurate information; however, Thermo Fisher Scientific assumes no responsibility and will not be liable for any errors, omissions, damage, or loss that might result from any use of this manual or the information contained therein (even if this information is properly followed and problems still arise) This publication is not part of the Agreement of Sale between Thermo Fisher Scientific and purchaser of a Combustion EA system. In the event of any conflict between the provisions of this document and those contained in Thermo Fisher Scientifics Terms and Conditions, the provisions of Terms and Conditions shall govern. ii Consumables & Spare/Service Parts Catalog Thermo Fisher Scientific

Copyright The content of this manual is protected by copyright. All efforts have been made to ensure the accuracy of the contents of this manual. However should any errors be detected Thermo Fisher Scientific would greatly appreciate being informed of them. The above notwithstanding Thermo Fisher Scientific can assume no responsibility for any errors in this manual or their consequences. For more information, check our website at http://www.thermo.com/ Any use of this manual other than, intended by the producer, is prohibited without the prior written permission of Thermo Fisher Scientific 2001-2007, Copyright reserved by Thermo Fisher Scientific Delft, The Netherlands Thermo Fisher Scientific Consumables & Spare/Service Parts Catalog iii

Preface Section Your comments regarding this manual are encouraged and will be considered for inclusion in later editions. Please write, fax, or email comments Voltaweg 22 2627 BC, Delft The Netherlands Tel.: +31 (0)15 2571314 Fax.:+31 (0)15 2572297 EMail: support.elemental.nl@thermofisher.com (for technical questions and remarks) mailsupport.sid.nl@thermofisher.com Web: www.thermo.com (for questions and remarks about the user s guide) iv Consumables & Spare/Service Parts Catalog Thermo Fisher Scientific

Contents Disclaimer...ii Copyright...iii Preface Section...iv Chapter 1 Chapter 2 TS4000100 Total sulfur analyzer model 4000...1-1 Consumables and Spare Parts...2-1 Cool options solids 3000...2-1 Liquid samples...2-2 NeXYZ autosampler...2-3 Sample Introduction...2-4 Universal liquids module...2-4 Solids introduction module, cool option...2-5 Chapter 3 Chapter 4 Chapter 5 Chapter 6 Chapter 7 Chapter 8 Combustion...3-1 Furnace tube...3-1 Conditioning...4-1 Without sulfuric acid scrubber...4-1 TTS-Parts... Error! Bookmark not defined. Silica gel dryer...5-2 Service parts TS Analyzer...6-3 UV-fluorescence detector...6-3 Vacuum pump...6-4 Furnace...6-5 Furnace compartment...6-6 PCB boards...6-7 Mass Flow controller...6-8 Cool option solids, 3000...7-1 Cool block...7-1 Spare parts/consumable kits...8-1 Starterpackage TS4000...8-1 One year consumables kit...8-2 Notes/ Additions / Comments...8-3 Thermo Fisher Scientific Consumables & Spare/Service Parts Catalog 1-1

Table of figures...8-4 I-1-2 Consumables & Spare/Service Parts Catalog

Chapter 1 TS4000100 Total sulfur analyzer model 4000 Figure 1 2. Total sulfur analyzer with accessories 1 Total Sulfur analyzer with TTS Technology 2 Universal Liquids Module Tn/TS/TX 3 Introduction module; cool option solids-3000 4 NeXYZ sampler, extended head 250µL, 2 ml vials 1 TS4000101 1 MODUL0019 1 MODUL0020 1 NEXYZ3000 -- NeXYZ support slede 1 NEXYZ0002 Thermo Fisher Scientific Consumables & Spare/Service Parts Catalog 1-1

-- TS 4000 Data acquisition package 1 TS4000102 -- Validation package TS 4000 1 TS4000103 -- Starter package TS 4000 1 TS4000104 I-1-2 Consumables & Spare/Service Parts Catalog

Chapter 2 Consumables and Spare Parts Cool options solids 3000 Figure 2 3. Consumables and spare parts cool option solids 1 Quartz sample cup, cool option 1 PINJE0018 2 Pair of tweezers 1 PMECH0013 Thermo Fisher Scientific Consumables & Spare/Service Parts Catalog 2-1

Liquid samples Figure 2 4. Consumables and spare parts for the liquids applications 1 Syringe 100µL 71mm, PS5, GA22, EURO2 2 Needles, 71 mm, PS5, GA, 3pcs,EURO2 1 PGENE0002 3 PGENE0004 3 Septum diam. 12mm, 10 pieces 10 PANAL0025 4 Glass-fibre filters TS, 10 pieces 10 PGENE0052 I-2-2 Consumables & Spare/Service Parts Catalog

NeXYZ autosampler Figure 2 5. Consumables NeXYZ 1 Needle, 213 mm GA 22, PS3, 3 pieces 1 PGENE0060 2 Vial screw caps, 100piecs 1 ELS200003 3 Septa 7.7mm PTFE, 100 pcs 1 ELS300006 4 Vial 2 ml, 100 pieces 1 ELS200042 Thermo Fisher Scientific Consumables & Spare/Service Parts Catalog I-2-3

Sample Introduction Universal liquids module Figure 2 1. Universal liquids module 1 Universal liquids module 1 MODUL0019 2 Glasspart universal liquids module 1 CASSE0012 3 Screwcap SQ 13/7 1 PMECH0010 4 Septum, diameter 12mm, 10 pcs 10 PANAL0025 5 Elbow red. union 4mm x ¼ PTFE 1 PMECH0763 I-2-4 Consumables & Spare/Service Parts Catalog

Solids introduction module, cool option Figure 2 2. Solids introduction module, cool option 3000 1 Introduction module; cool option solids-3000 1 MODUL0020 2 Stopper with septum solids 1 MODUL0006 3 Boatguiding tube, cool option 1 MODUL0021 4 Clamp (fork) NS-2 1 PMECH0040 5 Boat positioner TN solids 1 MODUL0016 6 Quartz combustion boat, cool 1 MODUL0022 7 Elbow red. union 4mm x ¼ PTFE 1 PMECH0763 Thermo Fisher Scientific Consumables & Spare/Service Parts Catalog I-2-5

Chapter 3 Combustion Furnace tube Figure 3 1. Quartz furnace tube and furnace accessories 1 Quartz turbo furnace tube, model 3000 1 PANAL0126 2 KS Clamp with screw nr. 35 1 PMECH0279 3 Centreerplate, new model 1 PMECH0930 4 Midlock hook TG-4-L 1 PMECH0972 Thermo Fisher Scientific Consumables & Spare/Service Parts Catalog 3-1

Chapter 4 Conditioning Without sulfuric acid scrubber Figure 4 1. Gas conditioning without sulfuric acid scrubber 1 Glass connector ¼ pp scr 1 PANAL0162 2 KS Clamp with screw nr. 12 1 PMECH0006 3 Perma pure dryer 1 TN3000029 4 Inline filter 211-4 1 PANAL0134 5 Glass connector ext oxygen ¼ 1 PANAL0069 6 Red union D1/4 D04 PFA 1 PMECH0368 Thermo Fisher Scientific Consumables & Spare/Service Parts Catalog 4-1

Chapter 5 Parts TTS-technology Silica gel dryer Figure 5 1. Silica gel dryer 1 Screw cap with septum, GL45 1 PMECH0079 2 Silica gel bottle 1 PANAL0259 3 O-ring teflex FEP/Sil 1 PMECH0031 4 Support silica gel bottle 1 PMECH0978 5 Silica gel 1 CHEM0036 I-5-2 Consumables & Spare/Service Parts Catalog

Chapter 6 Service parts TS 4000 Analyzer UVfluorescence detector Figure 6 1. Total Sulfur UV-fluorescence detector 1 TS- UV bench 1 TS3000011 2 Chamber inlet (8211) 1 TS3000013 3 Photomultiplier tube (8391) 1 TS3000007 4 Flash lamp TS (8666) 1 TS3000006 5 Male 1/8 BSP x ¼ OD 1 PMECH0863 6 Lens mount assembly (8827) 1 TS3000019 7 Mirror block TS-UV detector 1 TS3000022 8 Lampsocket for UV lamp (8392) 1 TS3000016 Thermo Fisher Scientific Consumables & Spare/Service Parts Catalog I-6-3

Vacuum pump Figure 6 2. Vacuumpump 1 Vacuumpump 1 TN3000003 2 Connector nylon elbow ¼ x ¼ 1 PMECH0061 3 Union ¼ x ¼ OD Nylon 1 PMECH0060 4 In-line filters 1 TN3000030 I-6-4 Consumables & Spare/Service Parts Catalog

Furnace Figure 6 3. Furnace 3000 serie 1 Oven model 3000, incl frame 1 PMECH0383 2 Thermo couple oven 1200/3000 serie 1 PELEC0132 3 Terminal 2P porcelain for T.C 1 PELEC0133 4 Clixon 1000 C 1 PELEC0143 Thermo Fisher Scientific Consumables & Spare/Service Parts Catalog I-6-5

Furnace compartment Figure 6 4. Furnace compartment and fan for cool option 300 1 Oven model 3000, incl frame 1 PMECH0383 2 Fans tiger, 80x80 1 PELEC0061 3 Solid state relais 1 PELEC0031 4 Fan 12VDC 60x60x25 1 PELEC0042 I-6-6 Consumables & Spare/Service Parts Catalog

PCB boards Figure 6 5. Electronic boards 1 EDAK 1.6 1 PELEC638 2 PCB-power 3000 1 PELEC0634 3 TS-Slave board 1 PELEC0618 4 PCB Flasher Supply TS 1 TS3000005 5 Power supply 60/15 1 PELEC0616 Thermo Fisher Scientific Consumables & Spare/Service Parts Catalog I-6-7

Mass Flow controller Figure 6 6. Mass flow controller, 5 canals 1 Mass flow controller, 5 canals 1 PMECH0868 2 Elbow 5 x 4 mm 1 PMECH0882 I-6-8 Consumables & Spare/Service Parts Catalog

TTS technology Figure 6 7. Service parts TTS technology 1 Scolopendra 1 TS4000001 2 Ozonkiller 1 HIPER5013 3 Reduction union D1/4 D04 PFA 1 PMECH0368 4 Active carbon scrubber 1 PGENE0025 5 Shutt off valves 1 HIPER0311 6 Glass tee connection, TTS 1 PGLAS0672 Thermo Fisher Scientific Consumables & Spare/Service Parts Catalog I-6-9

Chapter 7 Cool option solids, 3000 Cool block Figure 7 1. Cool block and PCB Cool option solids 3000 1 Cool option solids, frees 1 PMECH0950 2 Sub-Assy Module support 1 PCAS02001 3 Fan cool unit 1 PELEC0656 4 PCB Cool option solids 3000 1 PELEC0666 5 Temperature sensor cool option solids 3000 1 PELEC0667 6 Peltier element 1 PELEC0281 7 Terminal 2P porcelain for T.C. 1 PELEC0133 Thermo Fisher Scientific Consumables & Spare/Service Parts Catalog 7-1

Chapter 8 Spare parts/consumable kits Starterpackage TS4000 Starterpackage TS 4000 1 TS4000104 -- Septum diameter 12 mm, 10 pieces 1 PANAL0025 -- Silica gel TS4000, 65 g 2 CHEM00036 -- Needle, 213 mm, GA22, PS3, 3 pieces 1 PGENE0060 -- Glass-fibre filter TS, 10 pieces 1 PGENE0052 -- Septa 7.7 mm PTFE, 100 pieces 1 ELS300006 -- Vial 2 ml, 100 pieces 1 ELS200042 -- Vial screw caps, 100 pieces 1 ELS200003 -- Quartz sample cup, cool option 3 PINJE0018 -- Syringe 100µL, 71mm PS5, GA22 1 PGENE0002 -- Needles 71mm, GA22, 3 pieces 1 PGENE0004 -- Pair of tweezers RVS 1 PMECH0013 Thermo Fisher Scientific Consumables & Spare/Service Parts Catalog 8-1

One year consumables kit One year spare parts kit TS 4000 1 TS4000105 -- Septum diameter 12 mm, 10 pieces 5 PANAL0025 -- Silica gel TS4000, 65 g 12 CHEM00036 -- Needle, 213 mm, GA22, PS3, 3 pieces 2 PGENE0060 -- Glass-fibre filter TS, 10 pieces 5 PGENE0052 -- Septa 7.7 mm PTFE, 100 pieces 10 ELS300006 -- Vial 2 ml, 100 pieces 10 ELS200042 -- Vial screw caps, 100 pieces 10 ELS200003 -- Syringe 100µL, 71mm PS5, GA22 1 PGENE0002 -- Needles 71mm, GA22, 3 pieces 2 PGENE0004 -- Needle, 120 mm. PS5, GA 22, 3 pieces -- Turbo combustion tube, model 3000 2 PGENE0030 1 PANAL0126 -- Perma pure dryer only 1 PGENE0032 I-8-2 Consumables & Spare/Service Parts Catalog

Notes/ Additions / Comments Thermo Fisher Scientific Consumables & Spare/Service Parts Catalog I-8-3

Table of figures Figure 1 1. TS 4000 analyzer...i Figure 1 2. Total sulfur analyzer with accessories...1-1 Figure 2 2. Consumables and spare parts cool option solids...2-1 Figure 2 3. Consumables and spare parts for the liquids applications2-2 Figure 2 5. Consumables NeXYZ...2-3 Figure 3 1. Universal liquids module...2-4 Figure 3 2. Solids introduction module, cool option 3000...2-5 Figure 4 1. Quartz furnace tube and furnace accessories...3-1 Figure 5 1. Gas conditioning without sulfuric acid scrubber...4-1 Figure 6 1. Silica gel dryer...5-2 Figure 7 1. Total Sulfur UV-fluorescence detector...6-3 Figure 7 2. Vacuumpump...6-4 Figure 7 3. Furnace 3000 serie...6-5 Figure 7 4. Furnace compartment and fan for cool option 300...6-6 Figure 7 5. Electronic boards...6-7 Figure 7 6. Mass flow controller, 5 canals...6-8 Figure 8 1. Cool block and PCB Cool option solids 3000...7-1 I-8-4 Consumables & Spare/Service Parts Catalog