GC/MS BATCH NUMBER: H20103
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1 GC/MS BATCH NUMBER: H20103 ESSENTIAL OIL: HELICHRYSUM ITALICUM BOTANICAL NAME: HELICHRYSUM ITALICUM ORIGIN: ITALY KEY CONSTITUENTS PRESENT IN THIS BATCH OF HELICHRYSUM ITALICUM OIL % α-pinene 34.1 NERYL ACETATE 22.9 γ-curcumene 8.6 ITALICENE 3.3 β-caryophyllene 2.4 α-selinene 2.2 LIMONENE 2.0 β-selinene 2.0 ar-curcumene 1.8 β-pinene 1.7 ITALIDIONE I 1.2 ISOITALICENE 1.2 Comments from Robert Tisserand: A wonderfully fresh, buttery Immortelle oil high in both a-pinene and neryl acetate, and 2% total italidiones nd St S. Twin Falls, ID * * planttherapy.com facebook.com/planttherapy * planttherapy.com/blog
2 Date : June 14, 2016 SAMPLE IDENTIFICATION Internal code : 16F09-PTH2-1-SM Customer identification : Helichrysum Italicum - Italy - H Type : Essential oil Source : Helychrisum italicum Customer : Plant Therapy ANALYSIS Method : PC-PA E06, "Analysis of the composition of a liquid essential oil by GC-FID" (in French). Analyst : Alexis St-Gelais, M. Sc., chimiste Analysis date : Checked and approved by : Alexis St-Gelais, M. Sc., chimiste Note: This report may not be published, including online, without the written consent from Laboratoire PhytoChemia. This report is digitally signed, it is only considered valid if the digital signature is intact. Page 1 of 6
3 IDENTIFIED COMPOUNDS Identification Column: BP5 Column: WAX R.T. R.I. % % R.I. R.T. Molecular Class 2-Methyl-3-pentanone Aliphatic ketone 2,4-Dimethyl-3-pentanone Aliphatic ketone 4-Methyl-3-hexanone Aliphatic ketone Heptanal Aliphatic aldehyde Tricyclene Monoterpene α-thujene * Monoterpene α-pinene [34.60] * Monoterpene α-fenchene Monoterpene Camphene Monoterpene Thuja-2,4(10)-diene * Monoterpene Sabinene [0.03] * Monoterpene β-pinene Monoterpene Myrcene 4.40* Monoterpene trans-dehydroxylinalool 4.40* 993 [0.17] Monoterp. ether oxide 6-Methyl-5-hepten-2-one Aliphatic ketone Δ3-Carene 4.67* Monoterpene α-phellandrene 4.67* 1009 [0.85] Monoterpene cis-dehydroxylinalool Monoterp. ether oxide α-terpinene Monoterpene para-cymene Monoterpene Limonene Monoterpene β-phellandrene * Monoterpene 1,8-Cineole [0.50] * Monoterp. ether cis-β-ocimene * Monoterpene trans-β-ocimene Monoterpene γ-terpinene [0.19] * Monoterpene Isobutyl angelate * Aliphatic ester Terpinolene Monoterpene para-cymenene Monoterpene 2,4-Dimethyl-heptane-3,5- dione Aliphatic ketone 2-Methylbutyl 2- methylbutyrate [0.21] * Aliphatic ester Linalool 6.67* Monoterp. alcohol Nonanal 6.67* 1114 [0.65] Aliphatic aldehyde endo-fenchol Monoterp. alcohol Camphor Monoterp. ketone Isoamyl angelate Aliphatic ester Borneol * Monoterp. alcohol Page 2 of 6
4 Terpinen-4-ol Monoterp. alcohol Dimethyl octanedione isomer * β-diketone 4,6-Dimethyl-3,5- octanedione β-diketone α-terpineol Monoterp. alcohol Decanal * Aliphatic aldehyde Unknown (m/z = 81, (53), 67 (49), 140 (47), 41 (44)) Neral * Monoterp. aldehyde 3-Methylamyl angelate [1.62] * Aliphatic ester Hexyl angelate [0.51] * Aliphatic ester α-terpinyl acetate [0.51] * Monoterp. ester α-ylangene Sesquiterpene Isoitalicene 17.36* [1.62] * Sesquiterpene α-copaene 17.36* 1363 [1.54] Sesquiterpene Neryl acetate * Monoterp. ester Geranyl acetate * Monoterp. ester Italicene Sesquiterpene β-caryophyllene Sesquiterpene β-gurjunene Sesquiterpene Aromadendrene [0.67] * Sesquiterpene Italidione I β-diketone β-acoradiene Sesquiterpene γ-selinene Sesquiterpene trans-β-farnesene [0.90] * Sesquiterpene Neryl propionate Monoterp. ester Germacrene D [0.51] * Sesquiterpene Italidione isomer β-diketone γ-curcumene 25.83* Sesquiterpene β-selinene 25.83* 1474 [10.47] Sesquiterpene α-selinene Sesquiterpene ar-curcumene [1.65] * Sesquiterpene Italidione II β-diketone α-muurolene Sesquiterpene γ-cadinene [23.80] * Sesquiterpene Italidione II isomer 28.56* β-diketone β-bisabolene 28.56* 1507 [0.73] Sesquiterpene β-curcumene 28.56* 1507 [0.73] Sesquiterpene δ-cadinene Sesquiterpene β-sesquiphellandrene Sesquiterpene Italicene ether Sesquiterp. ether Italidione III β-diketone Page 3 of 6
5 Italidione III isomer β-diketone Italidione III isomer II β-diketone Italidione III isomer III β-diketone Guaiol Sesquiterp. alcohol Rosifoliol analog? Sesquiterp. alcohol Neryl angelate? Monoterp. ester Selin-11-en-4-α-ol Sesquiterp. alcohol Total identified 97.39% 95.12% *: Two or more compounds are coeluting on this column [xx]: Duplicate percentage due to coelutions, not taken account in the identified total Note: no correction factor was applied OTHER DATA Physical aspect : Faintly yellow liquid Refractive index : ± (20 C) CONCLUSION No adulterant, contaminant or diluent were detected using this method. Page 4 of 6
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