Essential Validation Services

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Essential Validation Services

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1 Sample: Client: Sample: Batch # Artisan Aromatics CAS Number 8006-90-4 Type: Peppermint (Mentha x piperita) Peppermint Sample Report Essential Oil Conclusion: No adulterants, diluents, or contaminants were detected via this method. This oil meets the expected profile for genuine essential oil of Peppermint (Mentha X x piperita). Validated By: Phone: 317-361-5044 747 SW 2nd Ave, Gainesville, FL 32601 E-mail: Adam@essentialvalidationservices.com Summary of Analyses A fresh sample of Peppermint (Mentha x piperita) Essential Oil (10 ul in.5to.5 ml Hexane + ETOH) was prepared and analyzed via split injection GC/EI-MS. - This report may not be published without the consent of.

2 Main Compounds Percentages Menthol 31.43% Menthone 24.80% Menthofuran (Co-Eluting) 12.32% Menthyl acetate 7.59% 1,8-Cineole 4.76% Terpinen-4-ol 3.21% Limonene 2.34% Pulegone 1.77% beta-pinene 1.23% beta-caryophyllene 1.20% Germacrene D 1.15% alpha-pinene 0.85% Sabinene 0.52% Monoterpenes Sesquiterpenes Monoterpenols Sesquiterpenols Ketones 6.31% 3.89% 36.07% 0.07% 26.93% Esters Ethers Aldehydes Phenols Other 8.43% 17.08% 0.00% 0.00% 1.23% Monoterpenes Sesquiterpenes Monoterpenols Sesquiterpenols Ketones Esters Ethers Phenols Other - This report may not be published without the consent of.

3 - This report may not be published without the consent of.

4 Total Percentage 98.95% Peak Number RT Area % Compound Name RI Chemical Family 1 11.77 0.04% alpha-thujene 927.80 Monoterpene 2 11.99 0.85% alpha-pinene 936.10 Monoterpene 3 12.58 0.01% Camphene 950.30 Monoterpene 4 13.55 0.52% Sabinene 973.00 Monoterpene 5 13.65 1.23% beta-pinene 974.00 Monoterpene 6 13.91 0.02% 1-Octen-3-ol 980.00 Aliphatic Alcohol 7 13.98 0.01% Octan-3-one 981.00 Aliphatic Ketone 8 14.25 0.14% Myrcene 989.20 Monoterpene 9 14.49 0.15% 3-Octanol 992.00 Aliphatic Alcohol 10 14.75 0.05% alpha-phellandrene 1002.00 Monoterpene 11 15.21 0.23% alpha-terpinene 1014.00 Monoterpene 12 15.52 0.12% para-cymene 1024.30 Monoterpene 13 15.67 2.34% Limonene 1029.50 Monoterpene 14 15.75 4.76% 1,8-Cineole 1031.80 Monoterpene Ether 15 16.05 0.11% (Z)-beta-Ocimene 1037.80 Monoterpene 16 16.52 0.03% (E)-beta-Ocimene 1047.70 Monoterpene 17 16.82 0.50% gamma-terpinene 1054.00 Monoterpene 18 17.13 0.30% trans-sabinene hydrate 1072.00 Monoterpenol 19 17.98 0.14% Terpinolene 1092.10 Monoterpene 20 18.33 0.23% Linalool 1099.00 Monoterpenol 21 20.03 0.13% Isopulegol 1151.25 Monoterpenol 22 20.34 24.80% Menthone 1155.00 Monoterpene Ketone 23 20.68 12.32% Menthofuran 1164.00 Monoterpene Ether 24 20.68 Co-Eluting Isomenthone 1164.33 Monoterpene Ketone 25 20.68 Co-Eluting Neomenthol 1165.00 Monoterpenol 26 21.07 31.43% Menthol 1177.40 Monoterpenol 27 21.16 3.21% Terpinen-4-ol 1180.57 Monoterpenol 28 21.35 0.34% Isomenthol 1183.75 Monoterpenol 29 21.53 0.30% alpha-terpineol 1191.71 Monoterpenol 30 21.63 0.13% Neoisomenthol 1193.50 Monoterpenol 31 23.21 1.77% Pulegone 1244.43 Monoterpene Ketone 32 23.74 0.35% Piperitone 1258.50 Monoterpene Ketone 33 24.31 0.35% Neomenthyl acetate 1275.00 Monoterpene Ester 34 24.91 7.59% Menthyl acetate 1297.00 Monoterpene Ester 35 25.40 0.28% Isomenthyl acetate 1306.00 Monoterpene Ester 36 26.33 0.21% cis-carvyl acetate 1368.00 Monoterpene Ester 37 27.58 0.05% alpha-copaene 1379.00 Sesquiterpene 38 27.86 0.24% beta-bourbonene 1388.70 Sesquiterpene 39 28.01 0.17% beta-elemene 1389.20 Sesquiterpene 40 28.90 1.20% beta-caryophyllene 1427.14 Sesquiterpene 41 29.17 0.30% beta-copaene 1445.00 Sesquiterpene 42 29.61 0.12% (Z)-beta-Farnesene 1453.40 Sesquiterpene 43 29.89 0.18% alpha-humulene 1461.43 Sesquiterpene - This report may not be published without the consent of.

5 44 30.15 0.18% cis-muurola-4(14),5-diene 1465.75 Sesquiterpene 45 30.66 1.15% Germacrene D 1484.71 Sesquiterpene 46 31.10 0.19% Bicyclogermacrene 1490.71 Sesquiterpene 47 31.62 0.02% gamma-cadinene 1515.29 Sesquiterpene 48 31.81 0.09% delta-cadinene 1524.14 Sesquiterpene 49 33.80 0.07% Viridiflorol 1596.00 Sesquiterpenol - This report may not be published without the consent of.