Date : April 28, 2016 SAMPLE IDENTIFICATION Internal code : 16D12-GUR6-1-HM Customer identification : Invigorate - 7318 Type : Essential oil Source : Blend Customer : GuruNanda LLC. ANALYSIS Method : PC-PA-001-15E06, "Analysis of the composition of a liquid essential oil by GC-FID" (in French). Analyst : Alexis St-Gelais, M. Sc., chimiste Analysis date : 2016-04-25 Checked and approved by : Alexis St-Gelais, M. Sc., chimiste 2013-174 Note: This report may not be published, including online, without the written consent from Laboratoire PhytoChemia. This report is digitally signed, it is only considered valid if the digital signature is intact. Page 1 of 6
IDENTIFIED COMPOUNDS Identification Column: BP5 Column: WAX R.T. R.I. % % R.I. R.T. Molecular Class Tricyclene 3.13 916 0.02 0.02 929 0.82 Monoterpene α-thujene 3.22 921 0.01 0.03 957 0.93 Monoterpene α-pinene 3.32 927 0.38 0.33 949 0.90 Monoterpene Camphene 3.60 944 0.14 0.13 1004 1.13 Monoterpene 3-Methylcyclohexanone 3.94 965 0.04 0.06 1249 3.70 Aliphatic ketone Sabinene 4.02 969 0.24 0.24 1059 1.57 Monoterpene β-pinene 4.08 973 0.38 0.38 1042 1.43 Monoterpene Myrcene 4.35 990 0.68 0.63 1118 2.07 Monoterpene Octen-3-ol 4.42 994 0.02 0.01 1406 5.93 Aliphatic alcohol 6-Methyl-5-hepten-2-one 4.43 995 0.24 0.23 1281 4.13 Aliphatic ketone α-phellandrene 4.57 1003 0.01 0.01 1112 2.02 Monoterpene Octan-3-ol 4.63 1006 0.12 0.09 1354 5.17 Aliphatic alcohol Octanal 4.75 1013 0.10 0.09 1235 3.50 Aliphatic aldehyde α-terpinene 4.81 1016 0.06 0.05 1124 2.14 Monoterpene Limonene 5.08 1031 23.98 23.23 1148 2.42 Monoterpene 1,8-Cineole 5.12 1033 1.08 1.29 1150 2.45 Monoterp. ether cis-β-ocimene 5.21 1039 0.08 0.10 1190 2.92* Monoterpene trans-β-ocimene 5.39 1048 0.07 0.06 1206 3.09 Monoterpene γ-terpinene 5.57 1058 0.10 [0.10] 1190 2.92* Monoterpene cis-sabinene hydrate 5.87 1075 0.10 0.10 1414 6.06 Monoterp. alcohol 4-Nonanone 5.93 1078 0.13 0.12 1275 4.06 Aliphatic ketone Terpinolene 6.04 1084 0.06 0.04 1226 3.37 Monoterpene para-cymenene 6.25 1096 0.02 0.01 1377 5.51 Monoterpene Linalool 6.44 1105 0.22 0.24 1509 7.88 Monoterp. alcohol Nonanal 6.49 1107 0.02 0.01 1346 5.06 Aliphatic aldehyde Octen-3-yl acetate 6.54 1109 0.02 0.02 1341 4.99 Aliphatic ester trans-pinocarveol 7.30 1137 0.02 0.04 1580 9.97 Monoterp. alcohol Camphor 7.58 1148 0.06 0.03 1433 6.41 Monoterp. ketone Menthone 7.77* 1155 4.19 4.12 1395 5.77 Monoterp. ketone Citronellal 7.77* 1155 [4.19] 1.08 1423 6.23* Monoterp. aldehyde Menthofuran 7.89 1159 0.64 0.64 1412 6.03 Monoterp. ether Isomenthone 8.00 1163 0.74 0.65 1416 6.11 Monoterp. ketone neo-menthol 8.14 1169 0.38 0.45 1536 8.62* Monoterp. alcohol (Z)-Isocitral 8.23 1172 0.09 0.03 1487 7.44 Monoterp. aldehyde Terpinen-4-ol 8.46* 1181 4.83 4.70 1533 8.52* Monoterp. alcohol Menthol 8.46* 1181 [4.83] 4.67 1578 9.91 Monoterp. alcohol (E)-Isocitral 8.59 1185 0.17 0.05 1514 7.97 Monoterp. aldehyde Isomenthol 8.71 1190 0.06 0.35 1561 9.40 Monoterp. alcohol neoiso-menthol 9.02 1201 0.11 0.10 1622 11.29 Monoterp. alcohol α-terpineol 9.12* 1204 0.12 0.12 1631 11.72 Monoterp. alcohol cis-dihydrocarvone 9.12* 1204 [0.12] 0.15 1534 8.55 Monoterp. ketone Page 2 of 6
Decanal 9.48 1212 0.10 0.06 1441 6.57 Aliphatic aldehyde trans-carveol 10.41 1233 0.02 0.06 1759 18.02 Monoterp. alcohol Neral 10.83 1242 5.15 5.18 1606 10.78 Monoterp. aldehyde Carvone 11.01 1247 9.14 15.10 1638 12.06* Monoterp. ketone Geraniol 11.33 1254 1.25 1.16 1786 19.69 Monoterp. alcohol neo-menthyl acetate 11.98 1269 0.04 0.04 1466 7.05 Monoterp. ester Geranial 12.25 1275 6.78 6.82 1656 12.80 Monoterp. aldehyde Menthyl acetate 12.90 1289 0.72 0.66 1503 7.75 Monoterp. ester Neryl acetate 16.64 1352 0.03 0.04 1674 13.62 Monoterp. ester α-copaene 17.10 1359 0.08 0.08 1426 6.30 Sesquiterpene β-patchoulene 17.41* 1364 1.12 [1.08] 1423 6.23* Sesquiterpene β-bourbonene 17.41* 1364 [1.12] 0.17 1456 6.87 Sesquiterpene β-elemene 18.25 1377 0.30 [0.45] 1536 8.62* Sesquiterpene Geranyl acetate 18.73 1384 0.60 0.67 1694 14.54 Monoterp. ester (Z)-Jasmone 19.54 1396 0.02 0.03 1844 23.28 Jasmonate β-caryophyllene 19.90 1402 1.95 2.05 1526 8.33 Sesquiterpene α-guaiene 21.49 1421 4.09 [4.70] 1533 8.52* Sesquiterpene Seychellene 21.75 1424 2.13 3.75 1549 9.04* Sesquiterpene α-humulene 22.67* 1436 1.90 0.27 1586 10.14 Sesquiterpene α-patchoulene 22.67* 1436 [1.90] [3.75] 1549 9.04* Sesquiterpene γ-patchoulene 22.89 1438 0.67 0.99 1552 9.11* Sesquiterpene δ-patchoulene 23.11 1441 0.32 [0.99] 1552 9.11* Sesquiterpene Germacrene D 24.71 1460 0.36 1.37 1628 11.56* Sesquiterpene Bicyclogermacrene 25.54 1470 0.25 [15.10] 1638 12.06* Sesquiterpene α-selinene 25.93 1475 0.11 [1.37] 1628 11.56* Sesquiterpene Aciphyllene 26.22 1478 0.80 [1.37] 1628 11.56* Sesquiterpene α-muurolene 26.39 1481 0.18 [15.10] 1638 12.06* Sesquiterpene δ-guaiene 26.77 1485 5.72 [15.10] 1638 12.06* Sesquiterpene Valencene 26.90 1487 0.15 0.21 1666 13.26* Sesquiterpene γ-cadinene 27.70* 1496 0.35 0.20 1670 13.46 Sesquiterpene β-bisabolene 27.70* 1496 [0.35] [0.21] 1666 13.26* Sesquiterpene Cubebol 28.02 1500 0.06 0.05 1854 24.04* Sesquiterp. alcohol δ-cadinene 28.36 1505 0.12 0.14 1676 13.72 Sesquiterpene Selina-3,7(11)-diene 29.29 1517 0.04 0.04 1679 13.87 Sesquiterpene Norpatchoulenol 31.90 1553 0.17 0.18 1973 31.85 Norsesquiterp. alcohol Caryophyllene oxide 32.75 1565 0.08 [0.05] 1854 24.04* Sesquiterp. ether γ-eudesmol 36.45 1625 0.06 0.06 2076 36.83 Sesquiterp. alcohol Pogostol 37.36 1647 3.07 0.75 2098 37.61 Sesquiterp. alcohol Patchoulol 37.45 1649 8.42 10.98 2029 35.18 Sesquiterp. alcohol Patchoulenone 39.24 1692 0.06 Sesquiterp. ketone Pogostone 40.04 1714 0.42 0.43 2339 43.92 Polyketone Nootkatone 42.60 1795 0.02 Sesquiterp. ketone Total identified 96.58% 96.24% *: Two or more compounds are coeluting on this column Page 3 of 6
[xx]: Duplicate percentage due to coelutions, not taken account in the identified total Note: no correction factor was applied OTHER DATA Physical aspect : Orange liquid Refractive index : 1.4850 ± 0.0003 (20 C) CONCLUSION Based on the analysis above, the listed ingredients for Invigorate are pure and natural. No adulterant, contaminant or diluent were detected using this method. Page 4 of 6
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