Essential Validation Services

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Essential Validation Services

Essential Validation Services

Essential Validation Services

Essential Validation Services

No adulterants, diluents, or contaminants were detected via this method. Conforms to 10/12 Iso Norms

No adulterants, diluents, or contaminants were detected via this method.

No adulterants, diluents, or contaminants were detected via this method.

No adulterants, diluents, or contaminants were detected via this method. Conforms to ranges found in the literature. Extra caution should be taken

Essential Validation Services

No adulterants, diluents, or contaminants were detected via this method. Total Italidione level 4-5%.

GC/MS BATCH NUMBER: TL0103

CERTIFICATE OF ANALYSIS - GC PROFILING

GC/MS BATCH NUMBER: R40106

GC/MS BATCH NUMBER: TL0101

GC/MS BATCH NUMBER: F80104

CERTIFICATE OF ANALYSIS GC PROFILING

GC/MS BATCH NUMBER: Y50101

GC/MS BATCH NUMBER: L50109

GC/MS BATCH NUMBER: LM0100

GC/MS BATCH NUMBER: S30103

GC/MS BATCH NUMBER: L40103

Alexis St-Gelais, M. Sc., chimiste

GC/MS BATCH NUMBER: B50105

GC/MS BATCH NUMBER: S40102

GC/MS BATCH NUMBER: F30105

GC/MS BATCH NUMBER: O50106

GC/MS BATCH NUMBER: CL0106

GC/MS BATCH NUMBER: CLO105

GC/MS BATCH NUMBER: BH0102

CERTIFICATE OF ANALYSIS - GC PROFILING

GC/MS BATCH NUMBER: SB5100

Alexis St-Gelais, M. Sc., chimiste

CERTIFICATE OF ANALYSIS - GC PROFILING

GC/MS BATCH NUMBER: EG0101

GC/MS BATCH NUMBER: CC0104

GC/MS BATCH NUMBER: CA0101

CERTIFICATE OF ANALYSIS - GC PROFILING

CERTIFICATE OF ANALYSIS - GC PROFILING

GC/MS BATCH NUMBER: R10104

GC/MS BATCH NUMBER: P40106

CERTIFICATE OF ANALYSIS - GC PROFILING

CERTIFICATE OF ANALYSIS - GC PROFILING

GC/MS BATCH NUMBER: P40105

CERTIFICATE OF ANALYSIS - GC PROFILING

GC/MS BATCH NUMBER: H90101

GC/MS BATCH NUMBER: CF0108

SAMPLE IDENTIFICATION ANALYSIS. Date : December 1, 2016

GC/MS BATCH NUMBER: H20103

Customer: Hemp Traders Type: Oil Instrument: UPLC-PDA-MS Submitted: 06/20/17

CERTIFICATE OF ANALYSIS - GC PROFILING

CERTIFICATE OF ANALYSIS - GC PROFILING

GC/MS BATCH NUMBER: E10106

GC/MS BATCH NUMBER: PJ0103

GC/MS BATCH NUMBER: PJ0102

GC/MS BATCH NUMBER: LU0100

GC/MS BATCH NUMBER: CD0103

GC/MS BATCH NUMBER: H20105

GC/MS BATCH NUMBER: CE0104

GC/MS BATCH NUMBER: G40105

GC/MS BATCH NUMBER: PJ0100

GC/MS BATCH NUMBER: CF0106

GC/MS BATCH NUMBER: TK0105

GC/MS BATCH NUMBER: W10104

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Transcription:

1 Sample: Client: Sample: Batch # Floracopia GPGROSVB01 CAS Number 8000-25-7 Type: Essential Oil Conclusion: No adulterants, diluents, or contaminants were detected via this method. This oil meets the expected profile for genuine oil of Rosemary (Rosmarinus X officinalis). Validated By: Phone: 317-361-5044 747 SW 2nd Ave, Gainesville, FL 32601 E-mail: Adam@essentialvalidationservices.com Summary of Analyses A fresh sample of (10 ul in.5to.5 ml Hexane + ETOH) was prepared and analyzed via split injection GC/EI-MS. - This report may not be published without the consent of.

2 Main Compounds Percentages alpha-pinene 15.49% Camphor 15.25% Bornyl acetate 13.45% Verbenone 10.06% 1,8-Cineole 9.38% Camphene 5.43% Borneol 4.09% Limonene 4.07% beta-pinene 2.07% Linalool 1.90% para-cymene 1.79% beta-caryophyllene 1.49% cis-pinocamphone 1.35% Monoterpenes Sesquiterpenes Monoterpenols Sesquiterpenols Ketones 33.92% 2.33% 10.85% 0.00% 27.58% Esters Ethers Aldehydes Phenols Other 13.57% 9.69% 0.00% 0.05% 2.01% Monoterpenes Sesquiterpenes Monoterpenols Sesquiterpenols Ketones Esters Ethers Phenols Other - This report may not be published without the consent of.

3 - This report may not be published without the consent of.

4 Total Percentage 98.05% Peak Number RT Area % Compound Name RI Chemical Family 1 12.14 0.02% Hashishene 922.00 Monoterpene 2 12.27 0.21% Tricyclene 923.00 Monoterpene 3 12.50 0.17% alpha-thujene 927.80 Monoterpene 4 12.80 15.49% alpha-pinene 936.10 Monoterpene 5 13.39 5.43% Camphene 950.30 Monoterpene 6 13.62 0.81% Thuja-2,4(10)-diene 953.00 Monoterpene 7 14.45 0.04% Sabinene 973.00 Monoterpene 8 14.57 2.07% beta-pinene 974.00 Monoterpene 9 14.97 0.01% Octan-3-one 981.00 Aliphatic Ketone 10 15.17 1.24% Myrcene 989.20 Monoterpene 11 15.73 0.21% alpha-phellandrene 1002.00 Monoterpene 12 15.97 0.03% delta-3-carene 1008.00 Monoterpene 13 16.24 0.34% alpha-terpinene 1014.00 Monoterpene 14 16.43 0.01% ortho-cymene 1021.33 Monoterpene 15 16.57 1.79% para-cymene 1024.30 Monoterpene 16 16.77 4.07% Limonene 1029.50 Monoterpene 17 16.88 9.38% 1,8-Cineole 1031.80 Monoterpene Ether 18 17.11 0.14% (Z)-beta-Ocimene 1037.80 Monoterpene 19 17.55 0.03% (E)-beta-Ocimene 1047.70 Monoterpene 20 18.00 0.80% gamma-terpinene 1054.00 Monoterpene 21 18.35 0.12% trans-sabinene hydrate 1072.00 Monoterpenol 22 18.56 0.01% cis-linalool oxide (5) (furanoid) 1075.10 Monoterpenol 23 19.02 0.03% Fenchone 1089.57 Monoterpene Ketone 24 19.22 1.02% Terpinolene 1092.10 Monoterpene 25 19.64 1.90% Linalool 1099.00 Monoterpenol 26 20.66 0.56% Chrysanthenone 1127.10 Monoterpene Ketone 27 21.29 0.15% trans-pinocarveol 1143.75 Monoterpenol 28 21.50 15.25% Camphor 1147.55 Monoterpene Ketone 29 21.62 0.07% trans-verbenol 1149.00 Monoterpenol 30 22.06 0.36% delta-terpineol 1166.00 Monoterpenol 31 22.30 4.09% Borneol 1168.71 Monoterpenol 32 22.59 1.35% cis-pinocamphone 1172.00 Monoterpene Ketone 33 22.70 1.15% Terpinen-4-ol 1180.57 Monoterpenol 34 23.21 1.14% alpha-terpineol 1191.71 Monoterpenol 35 23.46 0.85% Myrtenol 1198.00 Monoterpenol 36 23.68 0.71% beta-phellandren-8-ol 1199.00 Monoterpenol 37 23.95 10.06% Verbenone 1213.80 Monoterpene Ketone 38 24.21 0.06% trans-carveol 1223.14 Monoterpenol 39 24.91 0.17% Methyl thymol 1234.57 Monoterpene Ether 40 25.12 0.32% Carvone 1248.14 Monoterpene Ketone 41 26.12 0.24% trans-myrtanol 1258.00 Monoterpenol 42 26.66 13.45% Bornyl acetate 1288.29 Monoterpene Ester 43 27.08 0.12% Terpinen-4-yl acetate 1299.00 Monoterpene Ester - This report may not be published without the consent of.

5 44 28.78 0.01% alpha-terpinyl acetate 1353.00 Monoterpene Ether 45 29.76 0.01% alpha-copaene 1379.00 Sesquiterpene 46 30.19 0.66% beta-elemene 1389.20 Sesquiterpene 47 30.39 0.06% trans-jasmone 1392.00 Jasmonate 48 30.48 0.05% Methyl Eugenol 1407.27 Phenylpropanoid 49 31.24 1.49% beta-caryophyllene 1427.14 Sesquiterpene 50 32.31 0.17% alpha-humulene 1461.43 Sesquiterpene 51 36.27 0.13% Caryophyllene oxide 1594.86 Sesquiterpene Ether - This report may not be published without the consent of.