1 Sample: Client: Sample: Brambleberry Batch # 10355605 CAS Number 8000-28-0 Type: Lavender Absolute (Lavandula angustifolia) Essential Oil Conclusion: No adulterants, diluents, or contaminants were detected via this method. Conforms to ranges found in the literature. Extra caution should be taken X because of the levels of Coumarin and 7-methoxycoumarin. Validated By: Phone: 317-361-5044 Essential Validation Services 747 SW 2nd Ave, Gainesville, FL 32601 E-mail: Adam@essentialvalidationservices.com Summary of Analyses A fresh sample of Lavender Absolute (Lavandula angustifolia) Essential Oil (10 ul in.5to.5 ml Hexane + ETOH) was prepared and analyzed via split injection GC/EI-MS.
Main Compounds Lavender Absolute (Lavandula angustifolia) Percentages Coumarin 22.08% Linalyl acetate 15.76% Linalool 8.97% beta-caryophyllene 2.58% Lavandulyl acetate 2.47% Borneol 1.61% alpha-santalene 1.58% Geranyl acetate 1.40% Terpinen-4-ol 1.39% Camphor 1.28% 1,8-Cineole 1.25% Myrcene 0.68% Myrcene 0.68% Monoterpenes Sesquiterpenes Monoterpenols Sesquiterpenols Ketones 2.27% 7.05% 13.34% 4.12% 2.34% Esters Ethers Aldehydes Phenols Other 21.43% 2.66% 0.21% 0.00% 42.19% 2 Monoterpenes Sesquiterpenes Monoterpenols Sesquiterpenols Ketones Esters Ethers Phenols Other
3
4 Total Percentage 95.61% Peak Number RT Area % Compound Name RI Chemical Family 1 11.80 0.24% 1-Octen-3-ol 980.00 Aliphatic Alcohol 2 11.99 0.17% Octan-3-one 984.50 Aliphatic Ketone 3 12.12 0.68% Myrcene 989.20 Monoterpene 4 12.22 0.07% 3-Octanol 993.20 Aliphatic Alcohol 5 12.51 0.05% alpha-phellandrene 1004.10 Monoterpene 6 12.65 0.09% Hexyl acetate 1015.00 Aliphatic Ester 7 12.83 0.02% alpha-terpinene 1017.10 Monoterpene 8 13.03 0.07% para-cymene 1024.30 Monoterpene 9 13.15 0.21% Limonene 1029.50 Monoterpene 10 13.15 Co-Eluting beta-phellandrene 1030.00 Monoterpene 11 13.22 1.25% 1,8-Cineole 1031.80 Monoterpene Ether 12 13.30 0.34% (Z)-beta-Ocimene 1037.80 Monoterpene 13 13.56 0.48% (E)-beta-Ocimene 1047.70 Monoterpene 14 13.88 0.03% gamma-terpinene 1063.71 Monoterpene 15 14.21 0.35% cis-linalool oxide (5) (furanoid) 1075.10 Monoterpenol 16 14.59 0.36% trans-linalool oxide (5) (furanoid) 1092.20 Monoterpenol 17 14.84 8.97% Linalool 1099.00 Monoterpenol 18 14.94 0.08% Nonanal 1104.00 Aliphatic Aldehyde 19 15.02 0.60% Octen-3-yl acetate 1107.00 Aliphatic Ester 20 15.30 0.04% Octan-3-yl acetate 1117.50 Aliphatic Ester 21 15.48 0.39% Alloocimene 1129.90 Monoterpene 22 15.99 1.28% Camphor 1153.86 Monoterpene Ketone 23 16.36 0.36% Lavandulol 1161.50 Monoterpenol 24 16.46 1.61% Borneol 1168.71 Monoterpenol 25 16.68 1.39% Terpinen-4-ol 1180.57 Monoterpenol 26 16.82 0.37% UK (M/Z:43,56,67,71,82,89,91,115 27 16.89 0.68% Cryptone 1187.33 Monoterpene Ketone 28 16.95 0.15% alpha-terpineol 1191.71 Monoterpenol 29 17.38 0.21% Eucarvone 1214.00 Monoterpene Ketone 30 18.02 0.13% Cuminal 1243.00 Monoterpene Aldehyde 31 18.23 15.76% Linalyl acetate 1263.80 Monoterpene Ester 32 18.88 2.47% Lavandulyl acetate 1285.00 Monoterpene Ester 33 18.95 0.21% Bornyl acetate 1288.29 Monoterpene Ester 34 19.03 0.15% Cumin alcohol 1295.83 Monoterpenol 35 19.84 0.28% UK (M/Z:43,55,67,71,82,91,93,109 36 20.32 0.66% Neryl acetate 1362.90 Monoterpene Ester 37 20.68 1.40% Geranyl acetate 1370.10 Monoterpene Ester 38 20.94 0.43% Hydrocoumarin Isomer 39 21.59 1.58% alpha-santalene 1426.50 Sesquiterpene 40 21.70 2.58% beta-caryophyllene 1427.14 Sesquiterpene 41 21.86 0.39% trans-alpha-bergamotene 1435.00 Sesquiterpene 42 22.10 22.08% Coumarin 1433.00 Coumarin
5 43 22.66 0.21% Germacrene D 1484.71 Sesquiterpene 44 23.16 0.08% beta-bisabolene 1509.86 Sesquiterpene 45 23.35 1.51% gamma-cadinene 1515.29 Sesquiterpene 46 23.47 0.20% trans-calamenene 1529.50 Sesquiterpene 47 23.84 0.15% gamma-calacorene 1540.12 Sesquiterpene 48 24.18 1.19% Hydrocoumarin 49 24.64 1.41% Caryophyllene oxide 1594.86 Sesquiterpene Ether 50 25.50 4.12% T-Cadinol 1640.43 Sesquiterpenol 51 26.01 0.35% Cadalene 1666.00 Sesquiterpene 52 26.98 16.42% 7-methoxycoumarin 1743.00 Coumarin 53 28.12 0.38% UK (M/Z:43,65,69,77,79,93,109,12 54 29.40 0.48% UK (M/Z:43,69,79,91,109,119,135 55 30.27 0.25% UK (M/Z:41,55,69,77,93,105,119,1 56 32.67 0.20% Ethyl alpha-linolenate 2143.00 Fatty Acid Ester