GC/MS BATCH NUMBER: O50106 ESSENTIAL OIL: OREGANO ORGANIC BOTANICAL NAME: ORIGANUM VULGARE ORIGIN: MERSIN / TURKEY KEY CONSTITUENTS PRESENT IN THIS BATCH OF OREGANO ORGANIC OIL % CARVACROL 67.1 γ-terpinene 6.3 p-cymene 5.3 LINALOOL 4.3 β-bisabolene 1.7 MYRCENE 1.7 α-terpinene 1.6 α-thujene 1.1 β-caryophyllene 1.1 Comments from Robert Tisserand: Beautiful, if slightly unusual odor quality. This is due to higher than normal linalool content (4.4% against ISO standard of 0-3%). The other 10 key ISO constituents are within range. 510 2nd St S. Twin Falls, ID 83301 * 800-917-6577 * planttherapy.com facebook.com/planttherapy * planttherapy.com/blog
Date : November 15, 2017 SAMPLE IDENTIFICATION Internal code : 17K10-PTH4-1-CC Customer identification : Oregano Organic - Mersin / Turkey - O5010679R Type : Essential oil Source : Origanum vulgare Customer : Plant Therapy ANALYSIS Method : PC-PA-001-15E06, "Analysis of the composition of a liquid essential oil by GC-FID" (in French). Identifications double-checked by GC-MS Analyst : Sylvain Mercier, M. Sc., chimiste Analysis date : 2017-11-14 Checked and approved by : Alexis St-Gelais, M. Sc., chimiste 2013-174 Note: This report may not be published, including online, without the written consent from Laboratoire PhytoChemia. This report is digitally signed, it is only considered valid if the digital signature is intact. Page 1 of 5
IDENTIFIED COMPOUNDS Identification Column: BP5 Column: WAX R.T. R.I. % % R.I. R.T. Molecular Class Isovaleral 0.67 674 0.06 0.09 735 0.63* Aliphatic aldehyde 2-Methylbutyral 0.70 678 0.04 [0.09] 735 0.63* Aliphatic aldehyde Methyl 2-methylbutyrate 1.40 770 0.05 0.05 915 1.02* Aliphatic ester trans-2-hexenal 2.47 863 0.01 0.46 944 1.13* Aliphatic aldehyde cis-hex-3-en-1-ol 2.51 866 0.01 0.01 1340 5.77 Aliphatic alcohol Tricyclene 3.22 915 0.02 [0.05] 915 1.02* Monoterpene α-thujene 3.31 920 1.13 1.31 956 1.18 Monoterpene α-pinene 3.41 926 0.76 [0.46] 944 1.13* Monoterpene Camphene 3.70 943 0.32 0.26 998 1.42 Monoterpene β-pinene 4.19 972 0.15 0.12 1036 1.77 Monoterpene Myrcene 4.48* 989 2.21 1.66 1114 2.53 Monoterpene Octen-3-ol 4.48* 989 [2.21] 0.24 1394 6.60 Aliphatic alcohol Octan-3-one 4.51 991 0.26 5.29 1207 3.76* Aliphatic ketone α-phellandrene 4.75* 1004 0.40 0.18 1107 2.44 Monoterpene Δ3-Carene 4.75* 1004 [0.40] 0.09 1077 2.25 Monoterpene Octan-3-ol 4.81 1007 0.01 0.02 1351 5.93 Aliphatic alcohol α-terpinene 4.94 1015 1.56 2.07 1120 2.61 Monoterpene para-cymene 5.15 1026 5.27 [5.29] 1207 3.76* Monoterpene Limonene 5.17 1027 0.25 0.18 1138 2.85 Monoterpene β-phellandrene 5.20 1029 0.29 0.42 1143 2.92* Monoterpene 1,8-Cineole 5.23 1030 0.03 [0.42] 1143 2.92* Monoterp. ether cis-β-ocimene 5.34 1037 0.03 6.17 1188 3.50* Monoterpene trans-β-ocimene 5.52 1047 0.10 [5.29] 1207 3.76* Monoterpene γ-terpinene 5.74 1058 6.26 [6.17] 1188 3.50* Monoterpene cis-linalool oxide (fur.) 5.99 1072 0.02 0.02 1370 6.25 Monoterp. alcohol cis-sabinene hydrate 6.05 1075 0.31 0.33 1402 6.73* Monoterp. alcohol Terpinolene 6.19 1083 0.23 0.23 1222 3.98 Monoterpene trans-linalool oxide (fur.) 6.31 1089 0.02 [0.33] 1402 6.73* Monoterp. alcohol para-cymenene 6.41 1095 0.04 0.02 1363 6.12 Monoterpene Linalool 6.73* 1107 4.46 4.33 1491 8.84* Monoterp. alcohol trans-sabinene hydrate 6.73* 1107 [4.46] 0.13 1474 8.44 Monoterp. alcohol cis-para-menth-2-en-1-ol 7.22 1125 0.05 [4.33] 1491 8.84* Monoterp. alcohol α-campholenal 7.26 1127 0.05 Monoterp. aldehyde trans-para-menth-2-en-1-ol 7.74 1144 0.04 0.05 1560 11.23 Monoterp. alcohol Borneol 8.64 1177 0.73 1.08 1612 13.26* Monoterp. alcohol Terpinen-4-ol 8.80 1182 0.68 0.92 1522 9.82* Monoterp. alcohol α-terpineol 9.46 1203 0.14 0.16 1626 13.97 Monoterp. alcohol Carvacrol methyl ether 10.95 1236 0.10 [0.92] 1522 9.82* Monoterp. ether Linalyl acetate 11.37 1245 0.34 0.34 1497 8.98 Monoterp. ester Geraniol 11.81 1255 0.15 0.12 1780 22.99 Monoterp. alcohol Thymol 15.13 1318 0.83 0.77 2099 39.81 Monoterp. alcohol Page 2 of 5
Carvacrol 16.13 1333 67.05 68.42 2119 40.44* Monoterp. alcohol α-terpinyl acetate 16.32 1336 0.27 [1.08] 1612 13.26* Monoterp. ester β-bourbonene 18.11 1363 0.04 0.04 1450 7.87 Sesquiterpene Carvacryl acetate 18.47 1369 0.14 Monoterp. ester β-caryophyllene 20.60 1400 1.05 0.84 1517 9.65 Sesquiterpene Aromadendrene 21.98 1417 0.17 [0.92] 1522 9.82* Sesquiterpene α-humulene 23.39 1434 0.05 0.06 1578 11.88 Sesquiterpene Viridiflorene 26.42 1470 0.08 [1.08] 1612 13.26* Sesquiterpene β-bisabolene 28.88 1499 1.69 1.68 1656 15.54 Sesquiterpene δ-cadinene 29.33 1505 0.06 0.08 1670 16.30 Sesquiterpene Caryophyllene oxide 33.79 1568 0.24 0.23 1847 27.69 Sesquiterp. ether Spathulenol 33.97 1571 0.13 0.13 2014 37.10 Sesquiterp. alcohol τ-cadinol 37.52 1637 0.18 0.20 2068 38.83 Sesquiterp. alcohol α-cadinol 38.07 1651 0.03 [68.42] 2119 40.44* Sesquiterp. alcohol Shyobunol 39.43 1684 0.03 0.02 2207 42.70 Sesquiterp. alcohol Manoyl oxide 47.65 1968 0.02 0.03 2193 42.36 Diterp. ether Total identified 98.64% 98.85% *: Two or more compounds are coeluting on this column [xx]: Duplicate percentage due to coelutions, not taken account in the identified total Note: no correction factor was applied OTHER DATA Physical aspect : Light orange liquid Refractive index : 1.5048 ± 0.0003 (20 C) CONCLUSION No adulterant, contaminant or diluent were detected using this method. Page 3 of 5
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