GC/MS BATCH NUMBER: LM0100

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Transcription:

GC/MS BATCH NUMBER: LM0100 ESSENTIAL OIL: LAVENDER FINE ORGANIC BOTANICAL NAME: LAVANDULA ANGUSTIFOLIA ORIGIN: FRANCE KEY CONSTITUENTS PRESENT IN THIS BATCH OF LAVENDER FINE ORGANIC OIL % LINALYL ACETATE 34.0 LINALOOL 31.8 β-caryophyllene 3.6 cis-β-ocimene 3.4 trans-β-ocimene 3.0 LAVANDULYL ACETATE 3.0 TERPINEN-4-OL 3.0 trans-β-farnesene 2.4 OCTAN-3-ONE 1.6 α-terpineol 1.1 Comments from Robert Tisserand: Has a very fine Lavender fragrance. Conforms to 11 of 13 key ISO constituents for "spontaneous lavender". The other 2 probably do conform, but not clear from the analysis. 510 2nd St S. Twin Falls, ID 83301 * 800-917-6577 * planttherapy.com facebook.com/planttherapy * planttherapy.com/blog

Date : September 9, 2016 SAMPLE IDENTIFICATION Internal code : 16H30-PTH5-1-DM Customer identification : Org Lavender Fine - LM0100511R Type : Essential oil Source : Lavandula angustifolia Customer : Plant Therapy ANALYSIS Method : PC-PA-001-15E06, "Analysis of the composition of a liquid essential oil by GC-FID" (in French). Identifications double-checked by GC-MS Analyst : Alexis St-Gelais, M. Sc., chimiste Analysis date : 2016-08-30 Checked and approved by : Alexis St-Gelais, M. Sc., chimiste 2013-174 Note: This report may not be published, including online, without the written consent from Laboratoire PhytoChemia. This report is digitally signed, it is only considered valid if the digital signature is intact. Page 1 of 5

IDENTIFIED COMPOUNDS Identification Column: BP5 Column: WAX R.T. R.I. % % R.I. R.T. Molecular Class Isovaleral 0.53 567 0.01 0.02 778 0.49 Aliphatic aldehyde Hexanal 1.81 811 0.02 0.02 1007 1.11 Aliphatic aldehyde Methyl hexyl ether 1.88 817 0.09 0.08 847 0.60 Aliphatic ether cis-hex-3-en-1-ol 2.49 864 0.08 0.08 1321 4.61 Aliphatic alcohol Hexanol 2.70 881 0.14 0.15 1293 4.22 Aliphatic alcohol Tricyclene 3.16 913 0.02 0.02 927 0.79 Monoterpene α-thujene 3.25 918 0.07 0.07 953 0.89 Monoterpene α-pinene 3.35 924 0.16 0.15 945 0.86 Monoterpene Camphene 3.64 941 0.16 0.14 997 1.08 Monoterpene Sabinene 4.07 968 0.04 0.03 1055 1.49 Monoterpene β-pinene 4.13 971 0.06 0.05 1038 1.36 Monoterpene Myrcene 4.41 988 0.59 0.53 1115 1.98 Monoterpene Octan-3-one 4.46 991 1.55 1.40 1197 2.94* Aliphatic ketone Octen-3-ol 4.51 994 0.34 0.33 1398 5.73 Aliphatic alcohol Butyl butyrate 4.63 1001 0.10 Aliphatic ester Δ3-Carene 4.68* 1004 0.13 0.10 1088 1.75 Monoterpene α-phellandrene 4.68* 1004 [0.13] 0.02 1107 1.91 Monoterpene Octan-3-ol 4.77 1009 0.27 0.30 1347 5.00 Aliphatic alcohol Hexyl acetate 4.94 1018 0.45 0.53 1221 3.23* Aliphatic ester α-terpinene 4.97 1020 0.04 0.04 1121 2.05 Monoterpene meta-cymene 5.06 1025 0.15 0.27 1139 2.26* Monoterpene para-cymene 5.09* 1027 0.34 0.37 1207 3.05 Monoterpene Limonene 5.09* 1027 [0.34] [0.27] 1139 2.26* Monoterpene β-phellandrene 5.09* 1027 [0.34] 0.86 1143 2.32* Monoterpene 1,8-Cineole 5.15 1030 0.82 [0.86] 1143 2.32* Monoterp. ether cis-β-ocimene 5.29 1038 3.35 3.42 1186 2.81 Monoterpene trans-β-ocimene 5.47 1048 3.02 3.07 1203 3.00 Monoterpene γ-terpinene 5.64 1057 0.11 [1.40] 1197 2.94* Monoterpene cis-linalool oxide (fur.) 5.94 1073 0.19 0.20 1377 5.42 Monoterp. alcohol cis-sabinene hydrate 6.00 1076 0.05 0.09 1407 5.86 Monoterp. alcohol Terpinolene 6.11 1082 0.09 [0.53] 1221 3.23* Monoterpene trans-linalool oxide (fur.) 6.25 1090 0.16 0.12 1405 5.83 Monoterp. alcohol Linalool 6.78* 1112 32.74 66.53 1499 7.54* Monoterp. alcohol Octen-3-yl acetate 6.78* 1112 [32.74] 0.96 1332 4.77 Aliphatic ester Octan-3-yl acetate 6.97 1119 0.16 0.22 1297 4.29 Aliphatic ester Camphor 7.67 1145 0.37 0.29 1423 6.10 Monoterp. ketone Lavandulol 8.33 1170 0.93 0.92 1613 10.66 Monoterp. alcohol Borneol 8.61 1180 0.94 0.93 1619 10.86 Monoterp. alcohol Terpinen-4-ol 8.72 1184 2.98 6.75 1533 8.27* Monoterp. alcohol Hexyl butyrate 9.05* 1196 0.51 0.34 1372 5.35 Aliphatic ester Cryptone 9.05* 1196 [0.51] 0.26 1565 9.25 Monoterp. ketone Page 2 of 5

para-cymen-8-ol 9.16 1199 0.09 0.11 1766 17.72 Monoterp. alcohol α-terpineol 9.38 1204 1.14 1.93 1625 11.06* Monoterp. alcohol Nerol 10.64* 1232 0.24 0.20 1732 15.75 Monoterp. alcohol Bornyl formate 10.64* 1232 [0.24] 0.03 1462 6.84 Monoterp. ester Hexyl 2-methylbutyrate 10.64* 1232 [0.24] Aliphatic ester Linalyl acetate 11.47* 1251 34.06 [66.53] 1499 7.54* Monoterp. ester Cuminal 11.47* 1251 [34.06] 0.06 1674 13.17 Monoterp. aldehyde Geraniol 11.86 1260 0.51 0.50 1783 18.68 Monoterp. alcohol Bornyl acetate 12.74 1279 0.11 0.24 1511 7.77 Monoterp. ester Lavandulyl acetate 13.10 1287 2.98 2.93 1551 8.85 Monoterp. ester Neryl acetate 17.65 1359 0.33 0.31 1662 12.62* Monoterp. ester Geranyl acetate 19.14 1382 0.61 0.57 1693 13.99 Monoterp. ester β-caryophyllene 20.30 1399 3.59 [6.75] 1533 8.27* Sesquiterpene α-santalene 20.64 1403 0.43 0.47 1521 7.95 Sesquiterpene trans-α-bergamotene 21.81 1417 0.13 [6.75] 1533 8.27* Sesquiterpene α-humulene 23.00 1432 0.09 0.09 1587 9.90 Sesquiterpene trans-β-farnesene 24.24 1447 2.35 1.92 1627 11.14 Sesquiterpene Germacrene D 25.22 1458 0.46 [1.93] 1625 11.06* Sesquiterpene γ-cadinene 28.25 1494 0.09 0.08 1672 13.08 Sesquiterpene β-bisabolene 28.44 1497 0.03 [0.31] 1662 12.62* Sesquiterpene Caryophyllene oxide 33.49 1566 0.33 0.29 1854 22.99 Sesquiterp. ether τ-cadinol 37.32 1637 0.07 0.08 2080 36.21 Sesquiterp. alcohol Total identified 98.87% 99.47% *: Two or more compounds are coeluting on this column [xx]: Duplicate percentage due to coelutions, not taken account in the identified total Note: no correction factor was applied OTHER DATA Physical aspect : Clear liquid Refractive index : 1.4588 ± 0.0003 (20 C) CONCLUSION No adulterant, contaminant or diluent were detected using this method. Page 3 of 5

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