Essential Validation Services

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Essential Validation Services

Essential Validation Services

Essential Validation Services

Essential Validation Services

No adulterants, diluents, or contaminants were detected via this method.

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Essential Validation Services

GC/MS BATCH NUMBER: S30103

No adulterants, diluents, or contaminants were detected via this method. Conforms to ranges found in the literature. Extra caution should be taken

GC/MS BATCH NUMBER: S40102

No adulterants, diluents, or contaminants were detected via this method. Total Italidione level 4-5%.

No adulterants, diluents, or contaminants were detected via this method.

GC/MS BATCH NUMBER: P40106

GC/MS BATCH NUMBER: P40105

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GC/MS BATCH NUMBER: TL0101

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GC/MS BATCH NUMBER: PJ0103

GC/MS BATCH NUMBER: F80104

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GC/MS BATCH NUMBER: R40106

GC/MS BATCH NUMBER: L50109

GC/MS BATCH NUMBER: L40103

CERTIFICATE OF ANALYSIS - GC PROFILING

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GC/MS BATCH NUMBER: B50105

GC/MS BATCH NUMBER: O50106

GC/MS BATCH NUMBER: SB5100

GC/MS BATCH NUMBER: E10106

GC/MS BATCH NUMBER: CF0108

GC/MS BATCH NUMBER: BH0102

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GC/MS BATCH NUMBER: CLO105

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GC/MS BATCH NUMBER: R10104

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GC/MS BATCH NUMBER: CE0104

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GC/MS BATCH NUMBER: CA0101

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1 Sample: Client: Sample: Batch # Artisan Aromatics CAS Number 8008-79-5 Type: Spearmint (Mentha Spicata) Spearmint Sample Report Essential Oil Conclusion: No adulterants, diluents, or contaminants were detected via this method. This oil meets the expected profile for genuine essential oil of Spearmint (Mentha X Spicata). Validated By: Phone: 317-361-5044 747 SW 2nd Ave, Gainesville, FL 32601 E-mail: Adam@essentialvalidationservices.com Summary of Analyses A fresh sample of Spearmint (Mentha Spicata) Essential Oil (10 ul in.5to.5 ml Hexane + ETOH) was prepared and analyzed via split injection GC/EI-MS. - This report may not be published without the consent of.

2 Main Compounds Percentages Carvone 60.96% Limonene 19.30% Myrcene 2.56% 1,8-Cineole 1.70% cis-dihydrocarvone 1.35% beta-pinene 1.05% beta-bourbonene 1.02% Terpinen-4-ol 0.94% alpha-pinene 0.85% Germacrene D 0.79% gamma-terpinene 0.60% beta-copaene 0.52% Monoterpenes Sesquiterpenes Monoterpenols Sesquiterpenols Ketones 25.81% 3.96% 2.52% 0.00% 63.22% Esters Ethers Aldehydes Phenols Other 0.56% 1.70% 0.00% 0.00% 2.23% Monoterpenes Sesquiterpenes Monoterpenols Sesquiterpenols Ketones Esters Ethers Phenols Other - This report may not be published without the consent of.

3 - This report may not be published without the consent of.

4 Total Percentage 98.39% Peak Number RT Area % Compound Name RI Chemical Family 1 10.68 0.06% 2,5-Diethyltetrahydrofuran 895.30 Furan 2 11.41 0.08% Hashishene 922.00 Monoterpene 3 11.76 0.06% alpha-thujene 927.80 Monoterpene 4 11.99 0.85% alpha-pinene 936.10 Monoterpene 5 12.58 0.01% Camphene 950.30 Monoterpene 6 13.54 0.47% Sabinene 973.00 Monoterpene 7 13.64 1.05% beta-pinene 974.00 Monoterpene 8 14.21 2.56% Myrcene 989.20 Monoterpene 9 14.39 0.39% 3-Octanol 992.00 Aliphatic Alcohol 10 14.73 0.22% alpha-phellandrene 1002.00 Monoterpene 11 15.20 0.25% alpha-terpinene 1014.00 Monoterpene 12 15.51 0.14% para-cymene 1024.30 Monoterpene 13 15.67 19.30% Limonene 1029.50 Monoterpene 14 15.76 1.70% 1,8-Cineole 1031.80 Monoterpene Ether 15 16.06 0.08% (Z)-beta-Ocimene 1037.80 Monoterpene 16 16.82 0.60% gamma-terpinene 1054.00 Monoterpene 17 17.12 0.35% trans-sabinene hydrate 1072.00 Monoterpenol 18 17.97 0.14% Terpinolene 1092.10 Monoterpene 19 18.39 0.12% Linalool 1099.00 Monoterpenol 20 18.50 0.05% 1-Octenyl-3 acetate 1107.00 Monoterpene Ester 21 19.17 0.09% Octan-3-yl acetate 1124.00 Aliphatic Ester 22 19.82 0.08% trans-pinocarveol 1143.75 Monoterpenol 23 20.23 0.20% Menthone 1155.00 Monoterpene Ketone 24 20.75 0.21% Isomenthone 1164.33 Monoterpene Ketone 25 20.97 0.13% Menthol 1177.40 Monoterpenol 26 21.12 0.94% Terpinen-4-ol 1180.57 Monoterpenol 27 21.60 0.27% alpha-terpineol 1191.71 Monoterpenol 28 21.78 1.35% cis-dihydrocarvone 1197.57 Monoterpene Ketone 29 22.06 0.16% trans-dihydrocarvone 1203.83 Monoterpene Ketone 30 22.60 0.33% trans-carveol 1223.14 Monoterpenol 31 23.03 0.30% cis-carveol 1232.25 Monoterpenol 32 23.52 60.96% Carvone 1248.14 Monoterpene Ketone 33 23.75 0.25% Piperitone 1258.50 Monoterpene Ketone 34 24.07 0.04% cis-carvone oxide 35 24.54 0.09% trans-carvone oxide 1277.00 Monoterpene Ketone 36 25.99 0.40% Dihydrocarvyl acetate 1330.50 Monoterpene Ester 37 27.06 0.02% cis-carvyl acetate 1368.00 Monoterpene Ester 38 27.57 0.08% alpha-copaene 1379.00 Sesquiterpene 39 27.86 1.02% beta-bourbonene 1388.70 Sesquiterpene 40 28.01 0.17% cis-jasmone 1390.00 Jasmonate 41 28.90 0.30% beta-caryophyllene 1427.14 Sesquiterpene 42 29.17 0.52% beta-copaene 1445.00 Sesquiterpene 43 29.61 0.27% (E)-beta-Farnesene 1456.29 Sesquiterpene - This report may not be published without the consent of.

5 44 29.78 0.47% (Z)-beta-Farnesene 1453.40 Sesquiterpene 45 29.88 0.31% alpha-humulene 1461.43 Sesquiterpene 46 30.15 0.14% cis-muurola-4(14),5-diene 1465.75 Sesquiterpene 47 30.66 0.79% Germacrene D 1484.71 Sesquiterpene 48 31.57 0.01% gamma-cadinene 1515.29 Sesquiterpene 49 31.79 0.05% delta-cadinene 1524.14 Sesquiterpene - This report may not be published without the consent of.