SERVICES TECHNICAL SERVICES ANALYTICAL EQUIPMENT

Transcription

1 Analytical Services

2 TECHNICAL n con unction ith Siebel nstitute aboratory Services, hite abs offers the industry s most complete range of brewing-related tests. Tests are conducted using the strictest standards employing methods prescribed by the American Society of re ing hemists and AOA. any countries re uire certified lab documentation for export of alcohol products and hite abs has several certified beer chemists on staff. he lab participates in uarterly chec sample service to assess accuracy and uality control ithin the lab hich allo s hite abs to be confident in the data e are providing our customers. hite abs conducts test and delivers results in a prompt manner, providing customers ith information that is both timely and accurate. ANALYTICAL EQUIPMENT Anton Paar Alcolyzer ME and Density Meter ME 5000 HazeQC ME Turbidity Meter Together, our Anton Paar Density Meter, Alcolyzer, and HazeQC meter will reliably determine the alcohol content in beer and spirits. Additonally, these highly complex instruments can determine specific gravity, extract values, attenuation, ph, color, calories and chill haze. Perkin Elmer Clarus 500 and TurboMatrix 110 Headspace Unit Our top of the line as hromatograph can analy e off avors such as diacetyl and 2,3 pentanedione. It can also detect esters and fusels such as isoamyl acetate, ethyl acetate, acetaldehyde, methanol, isobutanol and acetone. Perkins Elmer Flexar Our HPLC can analyze sugars, acids, caffeine and more. New methods are added monthly.

3 Analytical Services & Testing Beer Kombucha Malt / Adjuncts Wine / Mead / Cider Product Price Description LS3010 Methanol LS3410 Ethyl Acetate LS3450 Distillation Profile LS3600 Gluten LS4000 Free SO 2 LS4030 Malic Acid LS4040 Lactic Acid LS4050 YAN (Yeast Assimilable Nitrogen) LS4060 Glucose/ Fructose $95.55 $66.15 $ $96.60 $16.80 $17.85 $33.60 $28.35 $17.85 Method: Gas Chromatograph. Results reported in ppm. Method: Gas Chromatograph. Results reported in ppm. includes ethyl acetate, 1-propanol, acetaldehyde, isoamyl alcohol, isoamyl acetate, acetone, ethyl butyrate, isobutyl acetate, methanol and isobutanol. Method: Gas Chromatograph. Results reported in ppm. Method: R5-Competitive Gliadin ELISA assay. Results reported in ppm. Method: Aeration oxidation. Results reported in mg/l. Analyze the amount of malic acid in wine before, during, or after malolactic fermentation. Method: Enzymatic. Results reported in mg/l. Method: Enzymatic. Results reported in mg/l. YAN is important when determining quality of must and how much nutrient addition is necessary. Method: Enzymatic. Results reporting in mg/l. Analyze wine for residual reducing sugars. Method: Enzymatic. Results report in g/l. LS4070 Testing for Wine & Cider LS4071 Juice $74.55 $57.75 includes titratable acidity, ph, SO 2, alcohol by volume, malic acid and Brix. Great panel for grape and apple must. includes titratable acidity, ph, Brix, YAN and malic acid testing. LS6600 Sediment $ Great test for issues with unusual haze or sediment in product. Typical analysis looks for dead yeast, alive yeast, oxalate crystals, protein and lipids. Sample is centrifuged and stained with Eosin Y and Thionin. Photos from microscopy and report of suspected sediments are included. LS6605 Full Process $ reat test to find out here contaminants are entering in your brewery. Test your entire process- Microbiological pre/post chiller, fermentors, brite tanks, hoses, rinse ater. fillers, bottles. etc. p to samples can be submitted. Includes WLD, LCSM, HLP and SDA selective media testing. Also includes ram stain and genus identification of any positive contaminants. LS6610 $ Includes WLD, LCSM, HLP and SDA Complete selective media testing. Also includes Gram stain Microbiological and genus identification of any positive contaminants.

4 eer ombucha alt Ad uncts ine ead ider Product Price Description LS6620 Complete S utritional abel LS6644 $ utritional eer LS6645 Calories LS6646 A V A $ $27.30 $27.30 LS6660 $14.70 rix LS6670 $ Sugar Profile by HP LS6671 $48.30 Viability LS Fat LS Genetic dentification S ixed ulture solation 6730 Saccharomyces cerevisiae. diastaticus S ombucha inal Product esting reat panel for a comprehensive loo at finished product. includes microbiological testing, S and H P selective medias, alcohol by volume and eight, extract values, attenuation, specific gravity, calories, ph, color,, diacetyl and, pentanedione. needed to create a nutritional label for your product. includes alcohol by volume and eight, extract values, attenuation, specific gravity, calories, ph, color, protein, total carbohydrates, cholesterol, total fat, calories from fat, trans fat, saturated fat, iron, calcium, sodium, sugar and dietary fiber. esults reported per. o. serving si e. includes alcohol by volume and eight, extract values, attenuation, specific gravity, calories, ph, color, protein and total carbohydrates. esults reported as calories o. Alcohol by volume and alcohol by eight. ethod Anton Paar eer Alcoly er and A default or as hromatograph. rix measured by Anton Paar ensity eter. includes glucose, fructose, lactose, maltose and sucrose. ethod HP. esults reported in percent. Viability analysis of yeast slurry. ethod methylene blue. ethod Acid hydrolysis. esults reported in percent. enetic se uencing of isolated bacteria or yeast. n most cases e are able to identify both genus and species of the organism. n bacteria, the S r A region is se uenced and for yeast, the S region is se uenced. esults ill be reported in a percent confidence level of the closest organism includes alcohol by volume via as hromatograph, titratable acidity, ph and total yeast and mold ml.

5 Beer Kombucha Malt / Adjuncts Wine / Mead / Cider Product Price Description S includes organic acid profile gluconic, acetic, Kombucha: lactic and malic acid), alcohol by volume via Gas Advanced Chromatograph, titratable acidity, ph, total yeast and Package mold (CFU/ml), total aerobic bacteria count (CFU/ml) and pathogens (Staphylococcus aureus, Enteric bacteria). LS6930 Kombucha: Shelf Life Testing $ includes alcohol by volume via Gas Chromatograph, titratable acidity, ph, total yeast and mold (CFU/ml), total aerobic bacteria count (CFU/ml) and CO 2 (if applicable). Testing is performed at 0, 30, 60, 90, 180 and 240 days. LS9014 Caffeine SIT0001 Fast Track Testing $ $ Method: HPLC. Results reported in percent. Get a range of our most requested services conducted on a fast-turnaround basis with accurate results sent back to you in 2 business days. includes alcohol by volume and weight, extract values, attenuation, specific gravity, calories, ph, color and. SIT0011 for Packaged Beer SIT0021 for Packaged Beer with Protein $ includes alcohol by volume and weight, extract values, attenuation, acidity, ph, SO 2, IBU, color, specific gravity, calories, O 2 and air. $210 includes alcohol by volume and weight, extract values, attenuation, acidity, ph, SO 2, IBU, color, specific gravity, calories, O 2, air and protein. SIT0031 lavor Profile SIT0033 Acetaldehyde SIT0040 $25.20 Titratable Acidity SIT0041 $25.20 Total Acidity SIT0050 $57.75 Alcohol, Extract and Calculated Values SIT0070 IBU Testing SIT0080 Calcium $ includes diacetyl, 2, 3 pentanedione, ethyl acetate, 1-propanol, acetaldehyde, isoamyl alcohol, isoamyl acetate, ethyl octanoate, ethyl hexanoate, acetone, methanol and isobutanol. Method: Gas Chromatograph. Results reported in ppm or ppb. $67.20 $40.95 $37.80 SIT0090 Total $69.30 Carbohydrates Method: Gas Chromatograph. Results reported in ppm. Method: Titration. Results reported in g/l. Method: Titration. Results reported in percent lactic acid. includes alcohol by volume and weight, calories, specific gravity, apparent extract, real extract, color, original extract, apparent attenuation, real degree attenuation and ph. Method: Anton Paar Alcolyzer and DMA5000. Method: Spectrophotometer. Results reported in BU (Bitterness Units). Method: ICP. Results reported in ppm. Method: ASBC calculation from extract, protein and ash. esults reported in g. o.

6 Beer Kombucha Malt / Adjuncts Wine / Mead / Cider Product Price Description SIT0091 Carbohydrate Sugar Profile by HPLC SIT0110 Chill Haze Testing $ This analysis gives a break down of the unfermentables (carbohydrates) in beer or wort samples. includes dextrins, maltriose, maltose, glucose and glycerol. Method: HPLC. Results reported in percent. $26.25 In this analysis one bottle is heated for one week to mimic one month of shelf life. Chill haze is analyzed at 4 C and reported from fresh and abused bottles. Method: Anton Paar Turbidity Meter. SIT0120 $49.35 Method: Zahm & Nagel piercing apparatus. CO 2 CO 2 and Air is reported in volumes and air is reported in cc. SIT0130 $26.25 Method: Anton Paar Alcolyzer or Color spectrophotometer. Results reported in SRM. SIT0140 $ Diacetyl. Method: Gas Chromatograph. Results reported in. SIT0141 $94.50 Diacetyl SIT0200 FAN $ Method: Gas Chromatograph. Results reported in. Free amino nitrogen. Method: Colormetric. Results reported in mg/l. SIT0270 ph SIT0291 Protein (Total) SIT0320 Total SO 2 $14.70 $54.60 $39.90 Acidity. Method: Spectrophotometer. Results reported in percent or g/12oz. Method: Enzymatic. Results reported in ppm. SIT0350 $78.75 Yeast Fermentable Extract (Y.F.E.) Helpful in determining the final gravity of a beer. Results reported in percent. SIT1000 Barley SIT3000 Moisture SIT3010 Alpha and Beta Acids SIT3060 Hop Oil Profile SIT3110 Total Essential Oils SIT4000 Malt $ includes moisture, protein, plumpness, kernel weight, germination energy, RVA and DON. $25.20 $59.85 $ $47.25 Moisture analysis of hops. Results reported in percent. Alpha and beta acids of hops. Method: HPLC. Results reported in percent. Volatile oil profile. include humulene, caryophyllene, myrcene, farnesene, linalool, geraniol and pinene. Results reported in percent. Total oil content in hops. Results reported in percent. $ includes moisture, assortment, friability, fine extract, coarse extract, F/C difference, β-glucan, FAN, soluble protein, S/T, diastatic power, α-amylase, color, filtration time and clarity.

7 Beer Kombucha Malt / Adjuncts Wine / Mead / Cider Product Price Description SIT4005 Basic Malt $ includes moisture, frability, fine extract, β-glucan, FAN, diastatic power, α-amylase, color, filtration time and clarity. SIT4010 Malt Enzyme SIT4015 Specialty Malt $78.75 $34.65 includes diastatic power and α-amylase. for high-dried, chocolate and roasted malt. includes moisture, extract and color. SIT6000 or Wort SIT9001 Zinc SIT9025 Iron $ includes ph, total dissolved solids, cations/ anions, sodium, potassium, calcium, magnesium, total hardness, nitrate, sulfate, chloride, carbonate, bicarbonate, total alkalinity, total phosphorus and total iron. $44.10 Method: ICP. Results reported in ppm. $59.85 Method: ICP. Results reported in ppm. Bundled Test Kits LSQCDayStandard Big QC Day Kit $139 Purchase this bundled kit and save! Test for diacetyl, IBUs, alcohol content, calories, SRM, attenuation (real and apparent), microbiological contaminants and more. Results depend on submission deadline and will be provided based on predetermined dates. To view dates visit whitelabs.com/bigqcday. This kit requires you to send your samples to White Labs in the provided sample bottle. Return FedEx shipping label is included. LSQCDayGluten Big QC Day Kit with Gluten Testing $199 All the same great tests and savings as LSQCDayStandard, plus analysis for gluten. Results depend on submission deadline and will be provided based on predetermined dates. To view dates visit whitelabs.com/bigqcday. This kit requires you to send your samples to White Labs in the provided sample bottle. Return FedEx shipping label is included.

8 ANALYSIS REQUEST FORM DATE: CUSTOMER INFORMATION COMPANY: CONTACT NAME: ADDRESS: PHONE: PAYMENT: CHECK P.O. CC NUMBER: EXP DATE: SAMPLE # PART NUMBER TEST NAME SAMPLE DESCRIPTION NOTES: Questions? AnalyticalLab@whitelabs.com Phone: ext 7387