ASTM D6042 Calibration Mixture
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1 Analytical Reference Materials ASTM D6042 Calibration Mixture Catalog # Lot # A & A Benner Circle Bellefonte, PA (814) FOR LABORATORY USE ONLY. READ MSDS PRIOR TO USE. RAW MATERIAL TEST INFORMATION AVAILABLE UPON REQUEST MANUFACTURED UNDER RESTEK'S ISO 9001 REGISTERED QUALITY SYSTEM
2 Certificate of Analysis 110 Benner Circle Bellefonte, PA Tel: (800) Fax: (814) FOR LABORATORY USE ONLY-READ MSDS PRIOR TO USE. Catalog No. : Lot No.: A Description : ASTM D6042 Calibration Mixture Expiration Date : April 2016 Storage: Refrigerate Elution Order CAS # Percent Purity 2 Concentration (weight/volume) 1 2,6-Di-tert-butyl-4-methylphenol (BHT) % 2 Erucamide % ug/ml 3 Irganox % 4 Irganox % 5 Vitamin E % 6 Irganox % 7 Irgafos % 3 % Uncertainty (95% C.L.; K=2) 4 Solvent: Isopropanol % Column: 150 mm x 4.6 mm Ultra C8 (cat.# ) Flow Rate: 1.5 ml/min. Mobile Phase A: H2O Mobile Phase B: Acetonitrile Mobile Phase 0 min.-75%b; 5 min.-100%b; 25 min. Det. Type: Wavelength: 200 nm Date Passed: 04/09/2009 Balance: Expiration date of the unopened ampule stored at recommended temperature. 2A Purity was determined by one or more of the following techniques: GC/FID, HPLC, GC/ECD, GC/MS. Value rounded to the nearest whole number. In addition to detectors listed above, chemical identity and purity are confirmed using one or more of the following: MS, DSC, solid probe MS, GC/FPD, GC/NPD, GC/TC, FTIR, melting point, refractive index, and Karl Fisher. See data pack or contact Restek for further details. 2B s with a listed purity of less than 99% have been weight corrected to compensate for impurities. 2C s with a listed purity of less than 99% may be salts, derivatives, or hydrates. The listed purity is actually a correction factor that was used to calculate the amount of compound necessary to acheive the desired concentration of the parent compound. 3 Based upon gravimetric preparation with balance calibration verified using NIST traceable weights (seven mass levels). 4 Uncertainties determined using repeatability and reproducibility data for balances and glassware from measurement systems analysis methodology, balance and glassware tolerances, raw material purity, and, where applicable, eccentricity and linearity values from an accredited calibration laboratory. Manufactured under Restek's ISO Registered Quality System Certificate #FMB0397
3 Catalog #: Target: 50 ug/ml Description: ASTM D6042 Calibration Mixture Solvent: Isopropanol Solvent Lot: Chemical Standard Batch Sheet Lot #:A Final Volume: 200 ml Made by: Joe Tallon Date: 3/25/ :43:28AM Tested by: Diane Shaffer Pass Date: 3/25/2009 2:23:37PM By: Diane Shaffer Date: 4/9/ :52:25AM Packaged by: Jessie Emel / Marty Rockey Date: 3/25/2009 1:08:48PM No. Units: 62 Pkg Size: 1 ml Balance Used: ARMBALPC2 XP205 Serial #: CAS Vitamin E Erucamide Irganox Irganox Irganox Irgafos ,6-Di-tert-butyl-4-methylphenol (BHT) Storage Target Location Lot # Purity Conc(ug/ml) Target Actual Calc Conc(ug/ml) RA2H13C 10209MQ mg mg RA2H13D 02024EY mg mg VL-001 HY8MZJJ mg mg VL-004 AB236E8U mg mg VL-006 AC256A8U mg mg VL-013 AA001A mg mg VL mg mg
4 Certificate of Analysis 110 Benner Circle Bellefonte, PA Tel: (800) Fax: (814) FOR LABORATORY USE ONLY-READ MSDS PRIOR TO USE. Catalog No. : Lot No.: A Description : ASTM D6042 Calibration Mixture Expiration Date : April 2017 Storage: Refrigerate Elution Order CAS # Percent Purity 2 Concentration (weight/volume) 1 2,6-Di-tert-butyl-4-methylphenol (BHT) % 2 Erucamide % ug/ml 3 Irganox % ug/ml 4 Irganox % 5 Vitamin E % 6 Irganox % 7 Irgafos % 3 % Uncertainty (95% C.L.; K=2) 4 Solvent: Isopropanol % Column: 150 mm x 4.6 mm Ultra C8 (cat.# ) Flow Rate: 1.5 ml/min. Mobile Phase A: H2O Mobile Phase B: Acetonitrile Mobile Phase Comp 0 min.-75%b; 5 min.-100%b; 25 min.-100%b Det. Type: Wavelength: 200 nm Date Passed: 08-Mar-2010 Balance: Expiration date of the unopened ampule stored at recommended temperature. 2A Purity was determined by one or more of the following techniques: GC/FID, HPLC, GC/ECD, GC/MS. Value rounded to the nearest whole number. In addition to detectors listed above, chemical identity and purity are confirmed using one or more of the following: MS, DSC, solid probe MS, GC/FPD, GC/NPD, GC/TC, FTIR, melting point, refractive index, and Karl Fisher. See data pack or contact Restek for further details. 2B s with a listed purity of less than 99% have been weight corrected to compensate for impurities. 2C s with a listed purity of less than 99% may be salts, derivatives, or hydrates. The listed purity is actually a correction factor that was used to calculate the amount of compound necessary to achieve the desired concentration of the parent compound. 2D Purity of isomeric compounds is reported as the sum of the isomers. Value is rounded to the nearest whole number after summation. 3 Based upon gravimetric preparation with balance calibration verified using NIST traceable weights (seven mass levels) and/or class A glassware used for dilutions. 4 Uncertainties determined using repeatability and reproducibility data for balances and glassware from measurement systems analysis methodology, balance and glassware tolerances, raw material purity, and, where applicable, eccentricity and linearity values from an accredited calibration laboratory. Manufactured under Restek's ISO 9001:2008 Registered Quality System Certificate #FM 80397
5 Catalog #: Target: 50 ug/ml Description: ASTM D6042 Calibration Mixture Solvent: Isopropanol Solvent Lot: Chemical Standard Batch Sheet Lot #:A Final Volume: 200 ml Made by: Matt Hepfer Date: 3/3/2010 6:28:08PM Tested by: Sara Eyster Pass Date: 3/4/2010 1:46:07PM By: Diane Shaffer Date: 3/8/2010 4:18:34PM Packaged by: Jessie Emel / cozzoli Date: 3/4/ :05:16AM No. Units: 139 Pkg Size: 1 ml Balance Used: ARMBALPC1 XP205 Serial #: CAS Vitamin E Erucamide Irganox Irganox Irganox Irgafos ,6-Di-tert-butyl-4-methylphenol (BHT) Storage Target Location Lot # Purity Conc(ug/ml) Target Actual Calc Conc(ug/ml) R MQ mg mg R EY mg mg VL-001 HY8MZJJ mg mg VL-004 AB236E8U mg mg VL-006 AC256A8U mg mg VL-013 AA001A mg mg VL mg mg
6 QA Report: ASTM D6042 Calibration Mixture (Cat.#31628) Runs of Lot # A Runs of Lot # A COMPONENT Run #1 Run #2 Run #3 AVG STD DEV % RSD Run #1 Run #2 Run #3 AVG STD DEV % RSD %D ME... P/F 2,6-Di-tert-butyl-4-methylphenol PASS Erucamide PASS Irganox PASS Irganox PASS Vitamin E PASS Irganox PASS Irgafos PASS 3/8/2010 4:15:28 PM 1/1-1
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