ELAP Certificate Numbers 1551 and January 2013
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1 ELAP Certificate Numbers 1551 and January 2013 PO Box / Attention SSC AP - CEMENT RE: Pond Discharge Work Order: 12K1305 Enclosed are the results of analyses for samples received by the laboratory on 11/30/12 21:00. If you have any questions concerning this report, please feel free to contact me. Sincerely, Sean Foley For Robbie C. Phillips Project Manager
2 Page 1 of 6 ANALYTICAL REPORT FOR SAMPLES Sample ID Laboratory ID Matrix Date Sampled Date Received Pond 30 (SD) 12K Water 11/30/12 12:15 11/30/12 21:00
3 Page 2 of 6 Pond 30 (SD) (12K ) METHOD Conventional Chemistry Parameters by APHA/EPA Methods Alpha Analytical Laboratories, Inc. BATCH PREPARED ANALYZED DILUTION RESULT PQL NOTE Sample Type: Water Sampled: 11/30/12 12:15 Oil & Grease (HEM) EPA 1664 AL /13/12 08:30 12/17/12 08:30 1 ND mg/l 5.0 ph SM4500-H+ B AL /30/12 13:10 11/30/12 17:23 " 8.25 ph Units 1.68 T-14 Specific Conductance (EC) SM2510B " " 11/30/12 17:27 " 1300 umhos/cm 20 Total Dissolved Solids SM2540C AL /03/12 10:30 12/06/12 13:15 " 900 mg/l 10 Total Suspended Solids SM2540D AL /05/12 07:24 12/11/12 12:41 " 82 " 1.0 Total Settleable Solids SM2540F AL /30/12 13:10 11/30/12 17:31 " 0.10 ml/l/hr 0.10 Total Organic Carbon SM5310C AL /13/12 09:44 12/14/12 18:37 " 3.33 mg/l 0.300
4 Page 3 of 6 Conventional Chemistry Parameters by APHA/EPA Methods - Quality Control Analyte(s) Spike Result PQL Units Level Source Result Limits Limit Flag Batch AL General Preparation Blank (AL20324-BLK1) Prepared: 12/03/12 Analyzed: 12/06/12 Total Dissolved Solids ND 10 mg/l Duplicate (AL20324-DUP1) Source: 12K Prepared: 12/03/12 Analyzed: 12/06/12 Total Dissolved Solids mg/l Duplicate (AL20324-DUP2) Source: 12K Prepared: 12/03/12 Analyzed: 12/06/12 Total Dissolved Solids mg/l Batch AL General Preparation Blank (AL20526-BLK1) Prepared: 12/05/12 Analyzed: 12/11/12 Total Suspended Solids ND 1.0 mg/l Duplicate (AL20526-DUP1) Source: 12L Prepared: 12/05/12 Analyzed: 12/11/12 Total Suspended Solids mg/l Duplicate (AL20526-DUP2) Source: 12K Prepared: 12/05/12 Analyzed: 12/11/12 Total Suspended Solids mg/l Batch AL General Preparation Duplicate (AL20619-DUP1) Source: 12K Prepared & Analyzed: 11/30/12 ph ph Units T-14 Specific Conductance (EC) umhos/cm
5 Page 4 of 6 Conventional Chemistry Parameters by APHA/EPA Methods - Quality Control Analyte(s) Spike Result PQL Units Level Source Result Limits Limit Flag Batch AL General Preparation Blank (AL21327-BLK1) Prepared: 12/13/12 Analyzed: 12/17/12 Oil & Grease (HEM) ND 5.0 mg/l LCS (AL21327-BS1) Prepared: 12/13/12 Analyzed: 12/17/12 Oil & Grease (HEM) mg/l LCS Dup (AL21327-BSD1) Prepared: 12/13/12 Analyzed: 12/17/12 Oil & Grease (HEM) mg/l Matrix Spike (AL21327-MS1) Source: 12L Prepared: 12/13/12 Analyzed: 12/17/12 Oil & Grease (HEM) mg/l 20.0 ND Batch AL General Prep Blank (AL21334-BLK1) Prepared: 12/13/12 Analyzed: 12/14/12 Total Organic Carbon ND mg/l LCS (AL21334-BS1) Prepared: 12/13/12 Analyzed: 12/14/12 Total Organic Carbon mg/l LCS Dup (AL21334-BSD1) Prepared: 12/13/12 Analyzed: 12/14/12 Total Organic Carbon mg/l Duplicate (AL21334-DUP1) Source: 12L Prepared: 12/13/12 Analyzed: 12/14/12 Total Organic Carbon mg/l Matrix Spike (AL21334-MS1) Source: 12L Prepared: 12/13/12 Analyzed: 12/14/12 Total Organic Carbon mg/l
6 Page 5 of 6 Conventional Chemistry Parameters by APHA/EPA Methods - Quality Control Analyte(s) Spike Result PQL Units Level Source Result Limits Limit Flag Batch AL General Prep Matrix Spike Dup (AL21334-MSD1) Source: 12L Prepared: 12/13/12 Analyzed: 12/14/12 Total Organic Carbon mg/l
7 Page 6 of 6 Notes and Definitions T-14 Residual chlorine, dissolved oxygen, and ph must be analyzed in the field to meet the EPA specified 15 minute hold time. Sample was received and analyzed outside of this "window." DET Analyte DETECTED ND NR dry PQL Analyte NOT DETECTED at or above the reporting limit Not Reported Sample results reported on a dry weight basis Relative Percent Difference Practical Quantitation Limit
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