No adulterants, diluents, or contaminants were detected via this method. Total Italidione level 4-5%.

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2 1 Sample: Client: Sample: Brambleberry Batch # CAS Number Type: Helichrysum Italicum (Helichrysum Italicum) Essential Oil Conclusion: No adulterants, diluents, or contaminants were detected via this method. Total Italidione level 4-5%. X Validated By: Phone: Essential Validation Services 747 SW 2nd Ave, Gainesville, FL Summary of Analyses A fresh sample of Helichrysum Italicum (Helichrysum Italicum) Essential Oil (10 ul in.5to.5 ml Hexane + ETOH) was prepared and analyzed via split injection GC/EI-MS.

3 Main Compounds Helichrysum Italicum (Helichrysum Italicum) Percentages gamma-curcumene 15.65% alpha-pinene 14.91% Neryl acetate 7.71% beta-selinene 6.95% Methyleugenol 6.43% beta-caryophyllene 4.75% Geranyl acetate 4.54% beta-bisabolene 4.07% Limonene 3.65% ar-curcumene 3.24% trans-α-bergamotene 2.92% Neryl propionate 1.94% Cedr-9-ene 1.59% Monoterpenes Sesquiterpenes Monoterpenols Sesquiterpenols Ketones 22.20% 44.40% 1.76% 6.31% 0.56% Esters Ethers Aldehydes Phenols Other 15.53% 1.78% 0.36% 6.43% 0.98% 2 Monoterpenes Sesquiterpenes Monoterpenols Sesquiterpenols Ketones Esters Ethers Phenols Other

4 3 RT: Time (min) NL: 1.52E8 TIC MS EVS-1188 Helichrysum 1

5 4 Total Percentage 99.96% Peak Number RT Area % Compound Name RI Chemical Family % alpha-pinene 6.10 Monoterpenes % alpha-fenchene Monoterpenes % Sabinene Monoterpenes % beta-pinene Monoterpenes % Myrcene Monoterpenes % alpha-phellandrene Monoterpenes % alpha-terpinene Monoterpenes % para-cymene Monoterpenes % Limonene Monoterpenes % 1,8-Cineole Ethers Co-Eluting beta-phellandrene Monoterpenes % (Z)-beta-Ocimene Monoterpenes % (E)-beta-Ocimene Monoterpenes % gamma-terpinene Monoterpenes % Terpinolene Monoterpenes % Linalool Monoterpenols % Nonanal Aldehydes % endo-fenchol Monoterpenols % 1-Terpineol Monoterpenols % Camphor Ketones % alpha-terpineol 1.71 Monoterpenols % alpha-terpinyl acetate Esters % Neryl acetate Esters % alpha-ylangene Sesquiterpenes % Geranyl acetate Esters Co-Eluting alpha-copaene Sesquiterpenes % beta-elemene Sesquiterpenes % Methyleugenol Phenols Co-Eluting Cedr-8-ene Sesquiterpenes % Cedr-9-ene Sesquiterpenes % beta-caryophyllene Sesquiterpenes % trans-α-bergamotene Sesquiterpenes % Neryl propionate Esters % Italidione I beta-diketone % gamma-selinene Sesquiterpenes % alpha-acoradiene Sesquiterpenes % beta-acoradiene Sesquiterpenes % gamma-curcumene Sesquiterpenes % ar-curcumene Sesquiterpenes % beta-selinene Sesquiterpenes Co-Eluting alpha-selinene Sesquiterpenes % beta-bisabolene Sesquiterpenes

6 Co-Eluting Italidione II beta-diketone % gamma-cadinene Sesquiterpenes % delta-cadinene Sesquiterpenes Co-Eluting Italidione II isomer beta-diketone % beta-sesquiphellandrene Sesquiterpenes % alpha-cadinene Sesquiterpenes Co-Eluting Italicene ether Ethers % (Z)-Nerolidol Sesquiterpenols % Italidione III beta-diketone % Spathulenol Sesquiterpenols Co-Eluting Italidione III isomer beta-diketone % Italidione III isomer II beta-diketone % Caryophyllene oxide Ethers % Guaiol Sesquiterpenols % Italidione isomer #N/A #N/A % Rosifoliol Sesquiterpenols % Geranyl isovalerate Esters % T-Cadinol Sesquiterpenols % beta-eudesmol Sesquiterpenols % Selin-11-en-4-α-ol Sesquiterpenols % alpha-eudesmol Sesquiterpenols % alpha-cadinol Sesquiterpenols % beta-bisabolol Sesquiterpenols

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