GC/MS BATCH NUMBER: BH0102

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1 GC/MS BATCH NUMBER: BH0102 ESSENTIAL OIL: BLUE TANSY ORGANIC BOTANICAL NAME: TANACETUM ANNUUM ORIGIN: MOROCCO KEY CONSTITUENTS PRESENT IN THIS BATCH OF BLUE TANSY ORGANIC OIL SABINENE ,9-DIHYDROCHAMAZULENE 11.8 % Comments from Robert Tisserand: The 12% of chamazulene is a good indicator of quality. CHAMAZULENE 12.1 CAMPHOR 7.3 α-phellandrene 4.1 MYRCENE 4.0 p-cymene 3.0 β-pinene 2.9 4,10-DIHYDROCHAMAZULENE 2.8 5,6-DIHYDROCHAMAZULENE 2.0 β-caryophyllene 1.9 BORNEOL 1.8 α-pinene 1.7 7,8-DIHYDROCHAMAZULENE 1.6 LIMONENE 1.5 1,8-CINEOLE 1.3 TERPINEN-4-OL 1.1 γ-terpinene nd St S. Twin Falls, ID * * planttherapy.com facebook.com/planttherapy * planttherapy.com/blog

2 Date : September 23, 2016 SAMPLE IDENTIFICATION Internal code : 16I16-PTH14-1-DM Customer identification : Organic Blue Tansy - BH010266R Type : Essential oil Source : Tanacetum annuum Customer : Plant Therapy ANALYSIS Method : PC-PA E06, "Analysis of the composition of a liquid essential oil by GC-FID" (in French). Analyst : Sylvain Mercier, M. Sc., chimiste Analysis date : Checked and approved by : Alexis St-Gelais, M. Sc., chimiste Note: This report may not be published, including online, without the written consent from Laboratoire PhytoChemia. This report is digitally signed, it is only considered valid if the digital signature is intact. Page 1 of 6

3 IDENTIFIED COMPOUNDS Identification Column: BP5 Column: WAX R.T. R.I. % % R.I. R.T. Molecular Class Ethyl 2-methylbutyrate Aliphatic ester Tricyclene Monoterpene α-thujene Monoterpene α-pinene Monoterpene α-fenchene 3.64* Monoterpene Camphene 3.64* 941 [0.67] Monoterpene Sabinene Monoterpene β-pinene Monoterpene Myrcene Monoterpene Octen-3-ol Aliphatic alcohol 6-Methyl-5-hepten-2-one Aliphatic ketone α-phellandrene 4.70* Monoterpene Δ3-Carene 4.70* 1005 [4.45] Monoterpene Octanal Aliphatic aldehyde α-terpinene Monoterpene para-cymene Monoterpene Limonene Monoterpene β-phellandrene * Monoterpene 1,8-Cineole [1.78] * Monoterp. ether cis-β-ocimene * Monoterpene trans-β-ocimene Monoterpene γ-terpinene [1.01] * Monoterpene cis-sabinene hydrate * Monoterp. alcohol Terpinolene Monoterpene Artemisia alcohol Monoterp. alcohol para-cymenene Monoterpene 6,7-Epoxymyrcene Monoterp. ether Linalool Monoterp. alcohol Nonanal Aliphatic aldehyde Unknown (m/z = 71, 43 (86), 81 (86), 79 (69), Oxygenated monoterpene (67), 41 (56), 53 (38) (7)) cis-para-menth-2-en-1-ol Monoterp. alcohol Limone ketone Monoterp. ketone trans-pinocarveol Monoterp. alcohol Camphor Monoterp. ketone Isoborneol Monoterp. alcohol Umbellulone Monoterp. ketone Borneol Monoterp. alcohol Terpinen-4-ol * Monoterp. alcohol Page 2 of 6

4 α-terpineol * Monoterp. alcohol α-phellandrene epoxide Monoterpene Decanal Aliphatic aldehyde Bornyl formate Monoterp. ester (Z)-Hex-3-en-1-yl Aliphatic ester isovalerate Pulegone Monoterp. ketone Cuminal Monoterp. aldehyde Thymol Monoterp. alcohol α-cubebene [0.25] * Sesquiterpene Carvacrol Monoterp. alcohol α-copaene Sesquiterpene β-elemene [1.83] * Sesquiterpene β-caryophyllene Sesquiterpene Aromadendrene [1.83] * Sesquiterpene cis-β-farnesene Sesquiterpene α-humulene Sesquiterpene allo-aromadendrene Sesquiterpene trans-β-farnesene [0.36] * Sesquiterpene Germacrene D Sesquiterpene β-selinene Sesquiterpene Bicyclogermacrene 26.41* Sesquiterpene α-selinene 26.41* 1472 [0.29] Sesquiterpene Valencene Sesquiterpene γ-cadinene Sesquiterpene 1,9-Dihydrochamazulene 29.01* Azulene δ-cadinene 29.01* 1504 [11.79] Sesquiterpene β-sesquiphellandrene Sesquiterpene 3,6-Dihydrochamazulene Azulene Spathulenol 33.48* Sesquiterp. alcohol Caryophyllene oxide 33.48* 1566 [0.33] Sesquiterp. ether 4,10-Dihydrochamazulene Azulene 5,6-Dihydrochamazulene Azulene γ-eudesmol Sesquiterp. alcohol 7,8-Dihydrochamazulene Azulene β-eudesmol Sesquiterp. alcohol α-cadinol Sesquiterp. alcohol α-bisabolol Sesquiterp. alcohol Chamazulene Azulene Unknown (m/z = 119, 121 (70), 105 (49), 93 (48), 91 (45), 109 (44), 41 (42) ?(4)) Diterpene Page 3 of 6

5 Unknown (m/z = 119, 121 (78), 132 (68), 93 (56) ? (2)) Unknown (m/z = 119, 132 (89), 109 (58), 145 (37), 105 (37) ?(4)) Diterpene Diterpene Total identified 91.44% 92.57% *: Two or more compounds are coeluting on this column [xx]: Duplicate percentage due to coelutions, not taken account in the identified total Note: no correction factor was applied OTHER DATA Physical aspect : Dark blue liquid Refractive index : N/A (too dark) CONCLUSION No adulterant, contaminant or diluent were detected using this method. Page 4 of 6

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