ICP Test Report Certification Packet

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1 ICP Certification Packet Company name: Littelfuse, Inc. Product Series: 3.6x10 Fuse Product #: 672P, 673P, 674P, 675P, 676P, 677P series Issue Date: April 26, 2014 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: [Global EHS Engineer] (1) Parts, sub-materials and unit parts This document covers the 3.6x10 Fuse RoHS-Compliant series products manufactured by Littelfuse, Inc. Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 Remarks 1 Form Rev. A 2/21/06

2 Table 1: List of Raw Materials covered by this report Item No. Raw Material Part Number Raw Material Description Page(s) 1 N/A Tinned Wires N/A Glass Fiber N/A Fuse Cap N/A Lead-free Solder N/A Body N/A Overcap/ Pigtail

3 RHS05F E 1 5 Report No. RHS05F E Page 1 of 5 Applicant CONQUER ELECTRONICS CO., LTD 26 Address NO.26, WUCYUAN 5TH ROAD., WUGU DISTRICT, NEW TAIPEI CITY, TAIWAN The following sample(s)and sample information was/were submitted and identified by/on the behalf of the client Sample Name TINNED COPPER ALLOY WIRE Part No Sample Received Date Dec.9, Testing Period Dec.9,2013 to Dec.11,2013 Test Requested (Pb)(Cd)(Hg) (Cr(VI)) As specified by client, to test Lead(Pb), Cadmium(Cd), Mercury(Hg),Hexavalent Chromium (Cr(VI)) in the submitted sample(s). Test Method Test Result(s) Please refer to following page(s). Please refer to following page(s). Tested by Reviewed by Approved by Date Su Hongwei Senior Laboratory Manager Centre Testing International Co.,Ltd. Shanghai Branch No No.1996,New Jinqiao Road, Pudong District,Shanghai,China

4 RHS05F E 2 5 Report No. RHS05F E Page 2 of 5 Test Method Tested Item(s) (Pb)/(Cd) Lead (Pb)/Cadmium (Cd) (Hg) Mercury (Hg) (Cr(VI)) Hexavalent Chromium (Cr(VI)) Test Method IEC 62321:2008 Ed.1 Sec.9 IEC 62321:2008 Ed.1 * Refer to IEC 62321:2008 Ed.1 * IEC 62321:2008 Ed.1 Sec.7 IEC 62321:2008 Ed.1 * Refer to IEC 62321:2008 Ed.1 * IEC 62321:2008 Ed.1Annex B Measured Equipment(s) ICP-OES ICP-OES UV-Vis Test Result(s) Tested Item(s) Result 1 2 MDL (Pb)Lead (Pb) N.D. 369 mg/kg 2mg/kg (Cd)Cadmium (Cd) N.D. N.D. 2mg/kg (Hg)Mercury (Hg) N.D. N.D. 2mg/kg (Cr(VI)) Hexavalent Chromium (Cr(VI)) / Tested Sample/Part Description 1. Metal base material 2. Grey plating :,, Note: : Negative Negative / -N.D. = (). -mg/kg=ppm=. -*= ICP-OES. - 50cm mg/kg The sample had been dissolved totally tested for Lead, Cadmium, Mercury. -MDL = Method Detection Limit -N.D. = Not Detected (<MDL ). - mg/kg = ppm =parts per million. -*=Appropriate acid is used for deplating, and the solution is analyzed by ICP OES. -Negative = Absence of Cr (VI). The Cr (VI) concentration detected in the boiling water extraction solution is less than 0.02 mg/kg with 50cm 2 sample surface area used. E Remark: The end sign of report number E represents the bilingual version.

5 RHS05F E 3 5 Report No. RHS05F E Page 3 of 5 Test Process 1. (Pb)/ (Cd) Lead (Pb)/ Cadmium (Cd) (1) IEC 62321:2008 Ed.1 Sec.9 Weigh sample and place it in a conical flask Add digestion reagent Digest the sample // ICP-OES Analyzed by ICP-OES Make up with deionized water Dry Ashing/ Alkali Fusion/ Acid Dissolution Residue Filtration Solution (2) IEC 62321:2008 Ed.1 * Take a portion of the sample Add digestion reagent Take out the substrate after the plating had been dissolved ICP-OES Analyzed by ICP-OES Make up with deionized water Transfer the plating digestive solution into a volumetric flask

6 RHS05F E 4 5 Report No. RHS05F E Page 4 of 5 2. (Hg) Mercury (Hg) (1) IEC 62321:2008 Ed.1 Sec.7 Weigh sample and place it in a microwave digestion vessel Add digestion reagent Digest sample in microwave digestion oven // ICP-OES Analyzed by ICP-OES Make up with deionized water Dry Ashing/ Alkali Fusion/ Acid Dissolution Residue Filtration Solution (2) IEC 62321:2008 Ed.1 * Take a portion of the sample Add digestion reagent Take out the substrate after the plating had been dissolved ICP-OES Analyzed by ICP-OES Make up with deionized water Transfer the plating digestive solution into a volumetric flask 3. (Cr(VI)) Hexavalent Chromium (Cr(VI)) Take a portion of the sample Extraction with boiling water Filter and remove the sample UV-Vis Analyzed by UV-Vis Add test solution ph Adjust the ph value of the solution

7 RHS05F E 5 5 Report No. RHS05F E Page 5 of 5 Photo(s) of the sample(s) RHS05F *** *** ***End of report *** The test report is effective only with both signature and specialized stamp. The result(s) shown in this report refer only to the sample(s) tested. Without written approval of CTI, this report can t be reproduced except in full.

8 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/12033* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

9 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/12033* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

10 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/12033* 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33 SGS Taiwan Ltd.

11 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/12033* 1) / These samples were dissolved totally by pre-conditioning method according to below flow chart.cr 6+ test method excluded 2) / Name of the person who made measurement: Climbgreat Yang 3) / Name of the person in charge of measurement: Troy Chang / CuttingPreparation / Sample Measurement Pb Cd ( ) / Acid digestion by suitable acid depended on different sample material (as below table) Hg // / Microwave digestion with HNO 3/HCl/HF Cr 6+ (Note**) /Add appropriate amount of digestion reagent / Solution / Filtration /Residue / Heat to appropriate temperature to extract /ICP-AES 1) / Alkali Fusion 2) / HCl to dissolve / Cool, filter digestate through filter / Sample Material / Digestion Acid,,, / Steel, copper, aluminum, solder,,,, / Aqua regia, HNO 3,HCl,HF,H 2O 2 /Glass, /HNO 3/HF,,, / / Aqua regia Gold, platinum, palladium, ceramic /Silver / HNO 3 / Plastic,,, / H 2SO 4,H 2O 2,HNO 3, HCl /Others / Added appropriate reagent to total digestion /Add diphenyl-carbazide for color development nm /measurethe absorbance at 540 nm by UV-VIS Note**(1) 90~95. / For non-metallic material, add alkaline digestion reagent and heat to 90~95. (2). / For metallic material, add pure water and heat to boiling. SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

12 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/12033* / PBB/PBDE analytical FLOW CHART / Name of the person who made measurement: Roman Wong / Name of the person in charge of measurement: Troy Chang / First testing process / Optional screen process / Confirmation process Sample / Sample pretreatment / Screen analysis / Sample extraction / Soxhlet method Concentrate/Dilute Extracted solution / Filter / AnalysisbyGC/MS/ Issue Report SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

13 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/12033* Analytical flow chart of halogen content / Name of the person who made measurement: Rita Chen / Name of the person in charge of measurement: Troy Chang / / Sample pretreatment/separation / Weighting and putting sample in cell / Oxygen Bomb Combustion / Absorption / Dilution to fixed volume / Analysis was performed by IC SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

14 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/12033* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

15 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2013/75138A* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

16 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2013/75138A* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

17 LIMA LIMA TECHNOLOGY CENTER, LIPA CITY, MALVAR, BATANGAS *CE/2013/75138A* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

18 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2013/75138A* 1) / These samples were dissolved totally by pre-conditioning method according to below flow chart. Cr 6+ test method excluded 2) / Name of the person who made measurement: Climbgreat Yang 3) / Name of the person in charge of measurement: Troy Chang /CuttingPreparation / Sample Measurement Pb Cd ( ) / Acid digestion by suitable acid depended on different sample material (as below table) Hg // / Microwave digestion with HNO 3/HCl/HF Cr 6+ (Note**) /Add appropriate amount of digestion reagent / Solution / Filtration / Residue / Heat to appropriate temperature to extract /ICP-AES 1) / Alkali Fusion 2) / HCl to dissolve /Cool, filter digestate through filter / Sample Material / Digestion Acid,,, / Steel, copper, aluminum, solder,,,, / Aqua regia, HNO 3, HCl, HF, H 2O 2 /Glass, / HNO 3/HF,,, / /Aquaregia Gold, platinum, palladium, ceramic /Silver / HNO 3 / Plastic,,, / H 2SO 4,H 2O 2, HNO 3, HCl /Others / Added appropriate reagent to total digestion /Add diphenyl-carbazide for color development nm /measurethe absorbance at 540 nm by UV-VIS Note**(1) 90~95. / For non-metallic material, add alkaline digestion reagent and heat to 90~95. (2). / For metallic material, add pure water and heat to boiling. SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

19 LIMA LIMA TECHNOLOGY CENTER, LIPA CITY, MALVAR, BATANGAS *CE/2013/75138A* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

20 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/20614A* 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33 SGS Taiwan Ltd.

21 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/20614A* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

22 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/20614A* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

23 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/20614A* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

24 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/20614A* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

25 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/20614A* 1) / These samples were dissolved totally by pre-conditioning method according to below flow chart. Cr 6+ test method excluded 2) / Name of the person who made measurement: Climbgreat Yang 3) / Name of the person in charge of measurement: Troy Chang /CuttingPreparation / Sample Measurement Pb Cd ( ) / Acid digestion by suitable acid depended on different sample material (as below table) Hg // / Microwave digestion with HNO 3/HCl/HF Cr 6+ (Note**) /Add appropriate amount of digestion reagent / Solution / Filtration / Residue / Heat to appropriate temperature to extract /ICP-AES 1) / Alkali Fusion 2) / HCl to dissolve /Cool, filter digestate through filter / Sample Material / Digestion Acid,,, / Steel, copper, aluminum, solder,,,, / Aqua regia, HNO 3, HCl, HF, H 2O 2 /Glass, / HNO 3/HF,,, / /Aquaregia Gold, platinum, palladium, ceramic /Silver / HNO 3 /Plastic,,, / H 2SO 4,H 2O 2, HNO 3, HCl /Others / Added appropriate reagent to total digestion /Add diphenyl-carbazide for color development nm /measurethe absorbance at 540 nm by UV-VIS Note** (For IEC 62321) (1) 90~95. / For non-metallic material, add alkaline digestion reagent and heat to 90~95. (2). / For metallic material, add pure water and heat to boiling. SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

26 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/20614A* 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33 SGS Taiwan Ltd.

27 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/20614A* PFOA/PFOS analytical flow chart / Name of the person who made measurement: Roman Wong / Name of the person in charge of measurement: Troy Chang Sample pretreatment Sample extraction by Ultrasonic extraction ( Reference method: US EPA 3550C) / Concentrate/Dilute Extracted solution Analysis was performed by LC/MS Data SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

28 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/20614A* / HBCDD analytical flow chart / Name of the person who made measurement: Roman Wong / Name of the person in charge of measurement: Troy Chang /Sample pretreatment Sample extraction / Ultrasonic method / Concentrate/Dilute Extracted solution / Filter / / Analysis was performed by GC/MS /Data 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33 SGS Taiwan Ltd.

29 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/20614A* Analytical flow chart of phthalate content / Name of the person who made measurement: Roman Wong / Name of the person in charge of measurement: Troy Chang / Sample pretreatment/separation Sample extraction by soxhlet method / Concentrate/Dilute Extracted solution Analysis was performed by GC/MS Data SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

30 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/20614A* Analytical flow chart of halogen content / Name of the person who made measurement: Rita Chen / Name of the person in charge of measurement: Troy Chang / / Sample pretreatment/separation / Weighting and putting sample in cell / Oxygen Bomb Combustion / Absorption / Dilution to fixed volume / Analysis was performed by IC 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33 SGS Taiwan Ltd.

31 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/20614A* / PBB/PBDE analytical FLOW CHART / Name of the person who made measurement: Roman Wong / Name of the person in charge of measurement: Troy Chang / First testing process / Optional screen process / Confirmation process Sample / Sample pretreatment / Screen analysis / Sample extraction / Soxhlet method Concentrate/Dilute Extracted solution / Filter / Analysis by GC/MS / Issue Report SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

32 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2014/20614A* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

33 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2013/C0811A* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

34 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2013/C0811A* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

35 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2013/C0811A* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

36 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2013/C0811A* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

37 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2013/C0811A* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

38 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2013/C0811A* 1) / These samples were dissolved totally by pre-conditioning method according to below flow chart.cr 6+ test method excluded 2) / Name of the person who made measurement: Climbgreat Yang 3) / Name of the person in charge of measurement: Troy Chang /CuttingPreparation / Sample Measurement Pb Cd ( ) / Acid digestion by suitable acid depended on different sample material (as below table) Hg // / Microwave digestion with HNO 3/HCl/HF Cr 6+ (Note**) /Add appropriate amount of digestion reagent / Solution / Filtration / Residue / Heat to appropriate temperature to extract /ICP-AES 1) / Alkali Fusion 2) / HCl to dissolve /Cool, filter digestate through filter / Sample Material / Digestion Acid,,, / Steel, copper, aluminum, solder,,,, / Aqua regia, HNO 3, HCl, HF, H 2O 2 /Glass, / HNO 3/HF,,, / /Aquaregia Gold, platinum, palladium, ceramic /Silver / HNO 3 /Plastic,,, / H 2SO 4,H 2O 2, HNO 3, HCl /Others / Added appropriate reagent to total digestion /Add diphenyl-carbazide for color development nm /measurethe absorbance at 540 nm by UV-VIS Note** (For IEC 62321) (1) 90~95. / For non-metallic material, add alkaline digestion reagent and heat to 90~95. (2). / For metallic material, add pure water and heat to boiling. SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

39 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2013/C0811A* / PBB/PBDE analytical FLOW CHART / Name of the person who made measurement: Roman Wong / Name of the person in charge of measurement: Troy Chang / First testing process / Optional screen process / Confirmation process Sample / Sample pretreatment / Screen analysis / Sample extraction / Soxhlet method Concentrate/Dilute Extracted solution / Filter / AnalysisbyGC/MS/ Issue Report SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

40 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2013/C0811A* PFOA/PFOS analytical flow chart / Name of the person who made measurement: Roman Wong / Name of the person in charge of measurement: Troy Chang Sample pretreatment Sample extraction by Ultrasonic extraction ( Reference method: US EPA 3550C) / Concentrate/Dilute Extracted solution Analysis was performed by LC/MS Data SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

41 LIMA LIMA TECHNOLOGY CENTER, LIPA CITY, MALVAR, BATANGAS *CE/2013/C0811A* Analytical flow chart of phthalate content / Name of the person who made measurement: Roman Wong / Name of the person in charge of measurement: Troy Chang / Sample pretreatment/separation Sample extraction by soxhlet method / Concentrate/Dilute Extracted solution Analysis was performed by GC/MS Data SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

42 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2013/C0811A* / HBCDD analytical flow chart / Name of the person who made measurement: Roman Wong / Name of the person in charge of measurement: Troy Chang /Sample pretreatment Sample extraction / Ultrasonic method / Concentrate/Dilute Extracted solution / Filter / / Analysis was performed by GC/MS /Data 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33 SGS Taiwan Ltd.

43 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2013/C0811A* Analytical flow chart of halogen content / Name of the person who made measurement: Rita Chen / Name of the person in charge of measurement: Troy Chang / / Sample pretreatment/separation / Weighting and putting sample in cell / Oxygen Bomb Combustion / Absorption / Dilution to fixed volume / Analysis was performed by IC 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33 SGS Taiwan Ltd.

44 LIMA LIMA TECHNOLOGY CENTER, LIPA LIPA CITY, MALVAR, BATANGAS *CE/2013/C0811A* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

45 LIMA LIMA TECHNOLOGY CENTER, LIPA CITY, MALVAR, BATANGAS *CE/2013/75141A* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

46 LIMA LIMA TECHNOLOGY CENTER, LIPA CITY, MALVAR, BATANGAS *CE/2013/75141A* 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33 SGS Taiwan Ltd.

47 LIMA LIMA TECHNOLOGY CENTER, LIPA CITY, MALVAR, BATANGAS *CE/2013/75141A* 1) / These samples were dissolved totally by pre-conditioning method according to below flow chart.cr 6+ test method excluded 2) / Name of the person who made measurement: Climbgreat Yang 3) / Name of the person in charge of measurement: Troy Chang /CuttingPreparation / Sample Measurement Pb Cd ( ) / Acid digestion by suitable acid depended on different sample material (as below table) Hg // / Microwave digestion with HNO 3/HCl/HF Cr 6+ (Note**) /Add appropriate amount of digestion reagent / Solution /Filtration /Residue / Heat to appropriate temperature to extract /ICP-AES 1) /AlkaliFusion 2) / HCl to dissolve /Cool, filter digestate through filter / Sample Material / Digestion Acid,,, / Steel, copper, aluminum, solder,,,, / Aqua regia, HNO 3, HCl, HF, H 2O 2 /Glass, / HNO 3/HF,,, / /Aquaregia Gold, platinum, palladium, ceramic /Silver / HNO 3 / Plastic,,, / H 2SO 4,H 2O 2, HNO 3, HCl /Others / Added appropriate reagent to total digestion /Add diphenyl-carbazide for color development nm /measurethe absorbance at 540 nm by UV-VIS Note**(1) 90~95. / For non-metallic material, add alkaline digestion reagent and heat to 90~95. (2). / For metallic material, add pure water and heat to boiling. SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

48 LIMA LIMA TECHNOLOGY CENTER, LIPA CITY, MALVAR, BATANGAS *CE/2013/75141A* SGS Taiwan Ltd. 33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 33

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